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Client Sample Results C Client: Geosyntec Consultants, Inc. TestAmerica Job ID: 320-47216-1 Project/Site: WR2501 Port of Stockton Client Sample ID: IDW-S-012819 Lab Sample ID: 320-47216-13 Date Collected: 01/28/19 15:00 Matrix: Solid Date Received: 01/29/19 16:35 Method: 8260B -Volatile Organic Compounds (GC/MS) (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,2-Dichlorobenzene ND 3.6 0.47 ug/Kg 02/01/1914:03 02/11/1913:40 1 1,3-Dichlorobenzene ND 3.6 0.22 ug/Kg 02/01/1914:03 02/11/1913:40 1 1,4-Dichlorobenzene ND 3.6 0.57 ug/Kg 02/01/1914:03 02/11/1913:40 1 Dichlorodifluoromethane ND 3.6 0.65 ug/Kg 02/01/1914:03 02/11/1913:40 1 1,1-Dichloroethane ND 3.6 0.21 ug/Kg 02/01/1914:03 02/11/1913:40 1 1,2-Dichloroethane ND 3.6 0.53 ug/Kg 02/01/1914:03 02/11/1913:40 1 1,1-Dichloroethene ND 3.6 0.19 ug/Kg 02/01/1914:03 02/11/1913:40 1 1,2-Dichloropropane ND 3.6 0.44 ug/Kg 02/01/1914:03 02/11/1913:40 1 1,3-Dichloropropane ND 3.6 0.42 ug/Kg 02/01/1914:03 02/11/1913:40 1 2,2-Dichloropropane ND 3.6 0.28 ug/Kg 02/01/1914:03 02/11/1913:40 1 1,1-Dichloropropene ND 3.6 0.27 ug/Kg 02/01/1914:03 02/11/1913:40 1 Ethylbenzene 15 3.6 0.25 ug/Kg 02/01/1914:03 02/11/1913:40 1 Hexachlorobutadiene ND 3.6 0.24 ug/Kg 02/01/1914:03 02/11/1913:40 1 Isopropyl benzene 9.3 3.6 0.38 ug/Kg 02/01/1914:03 02/11/1913:40 1 Methylene Chloride ND 7.3 0.61 ug/Kg 02/01/19 14:03 02/11/19 13:40 1 m-Xylene&p-Xylene 10 3.6 0.59 ug/Kg 02/01/19 14:03 02/11/19 13:40 1 Naphthalene 6.8 3.6 0.46 ug/Kg 02/01/1914:03 02/11/1913:40 1 n-Butylbenzene 12 3.6 0.48 ug/Kg 02/01/1914:03 02/11/1913:40 1 N-Propylbenzene 42 3.6 0.21 ug/Kg 02/01/1914:03 02/11/1913:40 1 o-Xylene 3.2 J 3.6 0.24 ug/Kg 02/01/1914:03 02/11/1913:40 1 p-Isopropyltoluene ND 3.6 0.46 ug/Kg 02/01/1914:03 02/11/1913:40 1 sec-Butyl benzene 4.6 3.6 0.55 ug/Kg 02/01/1914:03 02/11/1913:40 1 Styrene ND 3.6 0.23 ug/Kg 02/01/1914:03 02/11/1913:40 1 tert-Butylbenzene ND 3.6 0.39 ug/Kg 02/01/1914:03 02/11/1913:40 1 1,1,1,2-Tetrachloroethane ND 3.6 0.30 ug/Kg 02/01/1914:03 02/11/1913:40 1 1,1,2,2-Tetrachloroethane ND 3.6 0.50 ug/Kg 02/01/1914:03 02/11/1913:40 1 Tetrachloroethene ND 3.6 0.45 ug/Kg 02/01/1914:03 02/11/1913:40 1 Toluene 2.5 J 3.6 0.45 ug/Kg 02/01/1914:03 02/11/1913:40 1 trans-1,2-Dichloroethene ND 3.6 0.28 ug/Kg 02/01/1914:03 02/11/1913:40 1 trans-1,3-Dichloropropene ND 3.6 0.55 ug/Kg 02/01/1914:03 02/11/1913:40 1 1,2,3-Trichlorobenzene ND 3.6 0.55 ug/Kg 02/01/1914:03 02/11/1913:40 1 1,2,4-Trichlorobenzene ND 3.6 0.55 ug/Kg 02/01/1914:03 02/11/1913:40 1 1,1,1-Trichloroethane ND 3.6 0.26 ug/Kg 02/01/1914:03 02/11/1913:40 1 1,1,2-Trichloroethane ND 3.6 0.32 ug/Kg 02/01/1914:03 02/11/1913:40 1 Trichloroethene ND 3.6 0.44 ug/Kg 02/01/1914:03 02/11/1913:40 1 Trichlorofluoromethane ND 3.6 0.25 ug/Kg 02/01/1914:03 02/11/1913:40 1 1,2,3-Trichloropropane ND 3.6 0.55 ug/Kg 02/01/1914:03 02/11/1913:40 1 1,2,4-Tri methyl benzene 4.5 3.6 0.37 ug/Kg 02/01/1914:03 02/11/1913:40 1 1,3,5-Tri methyl benzene 1.9 J 3.6 0.26 ug/Kg 02/01/1914:03 02/11/1913:40 1 Vinyl chloride ND 3.6 0.26 ug/Kg 02/01/19 14:03 02/11/19 13:40 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene(Surr) 105 63-143 02/01/19 14:03 02/11/19 13:40 1 Dibromofluoromethane(Surr) 113 55-129 02/01/19 14:03 02/11/19 13:40 1 1,2-Dichloroethane-d4(Surr) 116 32-156 02/01/19 14:03 02/11/19 13:40 1 Toluene-d8(Surr) 109 63-138 02/01/19 14:03 02/11/19 13:40 1 Method: 8260B -Volatile Organic Compounds (GC/MS) - DL Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Bromomethane ND 84 10 ug/Kg 02/01/1914:27 02/11/1918:11 1 TestAmerica Sacramento Page 17 of 57 2/15/2019