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QC Sample Results C <br /> Client: Geosyntec Consultants, Inc. TestAmerica Job ID: 320-47216-1 <br /> Project/Site: WR2501 Port of Stockton <br /> Method: 82608 - Volatile Organic Compounds (GC/MS) (Continued) <br /> Lab Sample ID: LCSD 320-274191/28 Client Sample ID: Lab Control Sample Dup <br /> Matrix: Water Prep Type: Total/NA <br /> Analysis Batch: 274191 <br /> Spike LCSD LCSD %Rec. RPD <br /> Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit <br /> 2,2-Dichloropropane 20.0 25.3 ug/L 126 75-127 6 25 <br /> cis-1,3-Dichloropropene 20.0 20.6 ug/L 103 80-131 1 24 <br /> 1,1-Dichloropropene 20.0 20.3 ug/L 102 77-120 4 20 <br /> Ethylbenzene 20.0 19.5 ug/L 97 80-120 1 15 <br /> Hexachlorobutadiene 20.0 22.2 ug/L 111 69-120 2 30 <br /> Isopropylbenzene 20.0 20.0 ug/L 100 80-121 1 17 <br /> Methylene Chloride 20.0 21.5 ug/L 107 77-120 9 20 <br /> n-Butylbenzene 20.0 21.2 ug/L 106 72-120 1 25 <br /> Naphthalene 20.0 20.6 ug/L 103 56-143 11 48 <br /> N-Propylbenzene 20.0 19.8 ug/L 99 76-120 3 26 <br /> p-Isopropyltoluene 20.0 20.1 ug/L 100 76-120 5 18 <br /> sec-Butylbenzene 20.0 19.8 ug/L 99 77-120 4 19 <br /> Styrene 20.0 20.1 ug/L 101 80-120 1 15 <br /> tert-Butylbenzene 20.0 19.8 ug/L 99 78-120 3 19 <br /> 1,1,1,2-Tetrachloroethane 20.0 20.7 ug/L 103 79-120 2 23 ❑ <br /> 1,1,2,2-Tetrachloroethane 20.0 21.2 ug/L 106 74-137 1 27 <br /> Tetrachloroethene 20.0 19.1 ug/L 96 74-120 3 18 <br /> Toluene 20.0 19.8 ug/L 99 79-126 1 20 <br /> trans-1,2-Dichloroethene 20.0 19.5 ug/L 98 76-120 1 20 <br /> trans-1,3-Dichloropropene 20.0 20.6 ug/L 103 75-133 4 29 <br /> 1,2,3-Trichlorobenzene 20.0 18.8 ug/L 94 47-162 12 45 <br /> 1,2,4-Trichlorobenzene 20.0 20.2 ug/L 101 61-130 5 40 <br /> 1,1,1-Trichloroethane 20.0 20.3 ug/L 101 79-121 2 25 <br /> 1,1,2-Trichloroethane 20.0 20.3 ug/L 101 79-127 0 30 <br /> m-Xylene&p-Xylene 20.0 19.5 ug/L 97 80-121 1 15 <br /> Trichloroethene 20.0 18.9 ug/L 95 74-120 1 20 <br /> o-Xylene 20.0 19.9 ug/L 99 80-124 1 18 <br /> Trichlorofluoromethane 20.0 20.3 ug/L 102 60-135 1 41 <br /> 1,2,3-Trichloropropane 20.0 20.7 ug/L 104 73-120 3 22 <br /> 1,2,4-Trimethylbenzene 20.0 19.7 ug/L 98 76-120 2 17 <br /> 1,3,5-Trimethylbenzene 20.0 19.9 ug/L 99 79-120 2 20 <br /> Vinyl chloride 20.0 19.9 ug/L 100 68-121 1 33 <br /> LCSD LCSD <br /> Surrogate %Recovery Qualifier Limits <br /> 4-Bromofluorobenzene(Surr) 92 74-120 <br /> 1,2-Dichloroethane-d4(Surr) 93 72-123 <br /> Toluene-d8(Surr) 88 78-120 <br /> Dibromofluoromethane(Surr) 98 80-123 <br /> Lab Sample ID: MB 320-275295/6 Client Sample ID: Method Blank <br /> Matrix: Solid Prep Type: Total/NA <br /> Analysis Batch: 275295 <br /> MB MB <br /> Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac <br /> Benzene ND 5.0 0.26 ug/Kg 02/11/1911:17 1 <br /> Bromobenzene ND 5.0 0.52 ug/Kg 02/11/1911:17 1 <br /> Bromochloromethane ND 5.0 0.94 ug/Kg 02/11/1911:17 1 <br /> Bromodichloromethane ND 5.0 0.53 ug/Kg 02/11/1911:17 1 <br /> TestAmerica Sacramento <br /> Page 29 of 57 2/15/2019 <br />