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QC Sample Results C <br /> Client: Geosyntec Consultants, Inc. TestAmerica Job ID: 320-47216-1 <br /> Project/Site: WR2501 Port of Stockton <br /> Method: 82608 - Volatile Organic Compounds (GC/MS) (Continued) <br /> Lab Sample ID: LCS 320-275295/3 Client Sample ID: Lab Control Sample <br /> Matrix: Solid Prep Type: Total/NA <br /> Analysis Batch: 275295 <br /> Spike LCS LCS %Rec. <br /> Analyte Added Result Qualifier Unit D %Rec Limits <br /> Hexachlorobutadiene 50.0 60.6 ug/Kg 121 52-140 <br /> Isopropylbenzene 50.0 62.0 ug/Kg 124 69-137 <br /> Methylene Chloride 50.0 56.9 ug/Kg 114 77-125 <br /> n-Butylbenzene 50.0 63.2 ug/Kg 126 68-136 <br /> Naphthalene 50.0 51.0 ug/Kg 102 53-140 <br /> N-Propylbenzene 50.0 61.3 ug/Kg 123 63-128 <br /> p-Isopropyltoluene 50.0 61.0 ug/Kg 122 64-137 <br /> sec-Butylbenzene 50.0 62.6 ug/Kg 125 68-131 <br /> Styrene 50.0 57.5 ug/Kg 115 79-128 <br /> tert-Butylbenzene 50.0 61.4 ug/Kg 123 67-131 <br /> 1,1,1,2-Tetrachloroethane 50.0 57.3 ug/Kg 115 77-134 <br /> 1,1,2,2-Tetrachloroethane 50.0 54.1 ug/Kg 108 71-134 <br /> Tetrachloroethene 50.0 59.6 ug/Kg 119 65-135 <br /> Toluene 50.0 57.3 ug/Kg 115 80-124 <br /> trans-1,2-Dichloroethene 50.0 61.6 ug/Kg 123 67-135 ❑ <br /> trans-1,3-Dichloropropene 50.0 47.0 ug/Kg 94 80-148 <br /> 1,2,3-Trichlorobenzene 50.0 49.9 ug/Kg 100 54-140 <br /> 1,2,4-Trichlorobenzene 50.0 54.4 ug/Kg 109 48-145 <br /> 1,1,1-Trichloroethane 50.0 63.8 ug/Kg 128 67.150 <br /> 1,1,2-Trichloroethane 50.0 50.7 ug/Kg 101 80-128 <br /> m-Xylene&p-Xylene 50.0 59.8 ug/Kg 120 73-128 <br /> Trichloroethene 50.0 56.8 ug/Kg 114 80-126 <br /> o-Xylene 50.0 60.9 ug/Kg 122 76-127 <br /> Trichlorofluoromethane 50.0 64.6 ug/Kg 129 43-158 <br /> 1,2,3-Trichloropropane 50.0 54.3 ug/Kg 109 71-132 <br /> 1,2,4-Trimethylbenzene 50.0 58.8 ug/Kg 118 64-137 <br /> 1,3,5-Trimethylbenzene 50.0 61.1 ug/Kg 122 66-135 <br /> Vinyl chloride 50.0 54.9 ug/Kg 110 67-127 <br /> LCS LCS <br /> Surrogate %Recovery Qualifier Limits <br /> 4-Bromofluorobenzene(Surr) 106 63-143 <br /> 1,2-Dichloroethane-d4(Surr) 96 32-156 <br /> Toluene-d8(Surr) 108 63-138 <br /> Dibromofluoromethane(Surr) 104 55-129 <br /> Lab Sample ID: LCSD 320-275295/15 Client Sample ID: Lab Control Sample Dup <br /> Matrix: Solid Prep Type: Total/NA <br /> Analysis Batch: 275295 <br /> Spike LCSD LCSD %Rec. RPD <br /> Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit <br /> Benzene 50.0 58.9 ug/Kg 118 78-128 4 37 <br /> Bromobenzene 50.0 51.2 ug/Kg 102 67-132 5 40 <br /> Bromochloromethane 50.0 49.8 ug/Kg 100 80-127 6 36 <br /> Bromodichloromethane 50.0 53.9 ug/Kg 108 80-137 6 37 <br /> Methyl tert-butyl ether 50.0 50.1 ug/Kg 100 66-146 6 45 <br /> Bromoform 50.0 44.8 ug/Kg 90 80-136 16 45 <br /> Carbon tetrachloride 50.0 66.5 ug/Kg 133 62-154 5 43 <br /> Chlorobenzene 50.0 53.0 ug/Kg 106 74-125 4 38 <br /> TestAmerica Sacramento <br /> Page 32 of 57 2/15/2019 <br />