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Report Date: 06-Jun-2019 14:17:12 Chrom Revision: 2.3 02-Jun-2019 10:27:32 <br /> Eurofins TestAmerica, Sacramento <br /> Target Compound Quantitation Report <br /> Data File: \\chromna\Sacramento\ChromData\ATMS7\20190605-77431.b\MS7060522.D <br /> Lims ID: 320-50907-A-1 <br /> Client ID: 8468 <br /> Sample Type: Client <br /> Inject. Date: 06-Jun-2019 12:01:30 ALS Bottle#: 15 Worklist Smp#: 21 <br /> Purge Vol: 5.000 mL Dil. Factor: 1.0000 <br /> Sample Info: 320-50907-A-1 <br /> Misc. Info.: 500 mL CAN CERT <br /> Operator ID: LHS Instrument ID: ATMS7 <br /> Method: \\chromna\Sacramento\ChromData\ATMS7\20190605-77431.b\TO15_ATMS7N.m <br /> Limit Group: MSA-T01 - ICAL <br /> Last Update: 06-Jun-2019 14:16:59 Calib Date: 01-Jun-2019 22:53:30 <br /> Integrator: RTE ID Type: RT Order ID <br /> Quant Method: Internal Standard Quant By: Initial Calibration <br /> Last ICal File: \\chromna\Sacramento\ChromData\ATMS7\20190601-77232.b\MS70601 1 1.D <br /> Column 1 : RTX Volatiles(0.32 mm) Det: MS SCAN <br /> Process Host: CTX0308 <br /> First Level Reviewer: leeh Date: 06-Jun-2019 13:06:52 <br /> RT Adj RT Dlt RT OnCol Amt <br /> Compound Sig (min.) (min.) (min.) Q Response ppb v/v Flags <br /> * 1 Chlorobromomethane (IS) 130 12.268 12.353 -0.085 97 115376 10.0 <br /> * 21,4-Difluorobenzene 114 14.379 14.458 -0.079 96 466219 10.0 <br /> * 3 Chlorobenzene-d5 (IS) 117 21.010 21.077 -0.067 92 391003 10.0 <br /> $ 4 1,2-Dichloroethane-d4 (Sur 65 13.442 13.465 -0.086 98 231925 10.2 <br /> $ 5 Toluene-d8 (Surr) 100 17.744 17.734 -0.072 98 325428 9.77 <br /> $ 6 4-Bromofluorobenzene (Surr 95 23.553 23.566 -0.067 83 301564 9.69 m <br /> 32 Acetone 43 7.493 7.509 -0.061 98 12146 0.6727 <br /> 40 Carbon disulfide 76 8.837 8.882 -0.097 96 16509 0.6527 <br /> 73 n-Octane 43 17.737 17.770 -0.116 43 2721 0.0843 <br /> 1191,2,4-Trichlorobenzene 180 30.105 30.109 -0.073 0 2164 0.3365 <br /> Reagents: <br /> VAMSIS50_00011 Amount Added: 50.00 Units: mL Run Reagent <br /> Page 52 of 77 7/2/2019 <br />