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/--B McCampbell Analytical, Inc. "When Quality Counts" 1534 Willow Pass Road, Pittsburg, CA 94565-1701 Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269 http://www.mecampbell.com / E-mail: main@mceampbell.com Quality Control Report Client: Castle Analytical Laboratory WorkOrder: 2007D44 Date Prepared: 07/29/2020 BatchID: 202754 Date Analyzed: 07/29/2020 Extraction Method: E625.1 Instrument: GC21 Analytical Method: E625.1 Matrix: Water Unit: Project: 2007093/ 2007093/ Mizkan DRT 3297 / DRT 1026 Sample ID: MB/LCS/LCSD-202754 QC Summary Report for E625.1 Anatyte LCS Result LCSD Result SPK Val LCS %REC LCSD %REC LCS/LCSD Limits RPD RPD Limit Carbazole 9.13 8.74 10 91 87 70-130 4.31 25 n-Decane 8.38 8.54 10 84 85 50-130 1.88 25 n-Octadecane 8.99 8.47 10 90 85 70-130 5.93 25 Acenaphthene 0.430 0.411 0.50 86 82 70-130 4.55 25 Acenaphthylene 0.454 0.439 0.50 91 88 60-130 3.46 25 Anthracene 0.453 0.431 0.50 91 86 70-130 5.04 25 Benzidine 35.6 35.6 50 71 71 50-130 0.129 25 Benzo (a) anthracene 0.495 0.467 0.50 99 93 60-130 5.89 25 Benzo (a) pyrene 0.502 0.485 0.50 100 97 70-130 3.53 25 Benzo (b) fluoranthene 0.538 0.515 0.50 108 103 60-130 4.40 25 Benzo (g,h,i) perylene 0.444 0.423 0.50 89 85 70-130 4.79 25 Benzo (k) fluoranthene 0.473 0.454 0.50 95 91 70-130 4.10 25 Benzyl Alcohol 47.6 48.3 50 95 97 70-130 1.55 25 Bis (2-chloroethoxy) Methane 7.89 8.16 10 79 82 70-130 3.36 25 Bis (2-chloroethyl) Ether 0.413 0.422 0.50 83 84 60-130 2.15 25 Bis (2-chloroisopropyl) Ether 0.400 0.380 0.50 80 76 60-130 5.03 25 Bis (2-ethylhexyl) Adipate 9.14 8.56 10 91 86 60-130 6.63 25 Bis (2-ethylhexyl) Phthalate 0.511 0.474 0.50 102 95 60-130 7.55 25 4-Bromophenyl Phenyl Ether 11.8 11.2 10 118 112 70-130 4.94 25 Butylbenzyl Phthalate 0.484 0.450 0.50 97 90 60-130 7.18 25 4-Chloroaniline 0.464 0.476 0.50 93 95 70-130 2.52 25 4-Chloro-3-methylphenol 11.8 12.4 10 118 124 70-130 4.60 25 2-Chloronaphthalene 10.2 10.2 10 102 102 70-130 0.0737 25 2-Chlorophenol 0.405 0.422 0.50 81 84 60-130 4.02 25 4-Chlorophenyl Phenyl Ether 10.6 10.1 10 106 101 70-130 5.57 25 Chrysene 0.458 0.432 0.50 92 86 70-130 5.86 25 Dibenzo (a,h) anthracene 0.499 0.478 0.50 100 96 70-130 4.28 25 Dibenzofuran 8.87 8.72 10 89 87 70-130 1.67 25 Di-n-butyl Phthalate 0.501 0.471 0.50 100 94 70-130 6.19 25 1,2-Dichlorobenzene 10.2 10.6 10 102 106 60-130 3.89 25 1,3-Dichlorobenzene 9.17 9.64 10 92 96 60-130 4.98 25 1,4-Dichlorobenzene 9.03 9.24 10 90 92 60-130 2.31 25 3,3-Dichlorobenzidine 0.506 0.475 0.50 101 95 70-130 6.31 25 2,4-Dichlorophenol 0.519 0.535 0.50 104 107 70-130 2.96 25 2,6-Dichlorophenol 0.520 0.542 0.50 104 108 70-130 4.00 25 Diethyl Phthalate 0.475 0.448 0.50 95 90 70-130 5.89 25 2,4-Dimethylphenol 11.3 11.6 10 113 116 70-130 2.64 25 Dimethyl Phthalate 0.451 0.426 0.50 90 85 70-130 5.52 25 (Cont.) CA ELAP 1644 • NELAP 40330RELAP Page 20 of 30