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L <br />Analyst: JMH Reviewed by: BS <br />53.1 <br />26.6 <br />26.6 <br />26.6 <br />53.1 <br />5.31 <br />26.6 <br />26.6 <br />26.6 <br />26.6 <br />26.6 <br />26.6 <br />RL <br />5.31 <br />26.6 <br />26.6 <br />26.6 <br />26.6 <br />EMPC <br />2.94 <br />4.32 <br />4.70 <br />4.24 <br />5.74 <br />11.7 <br />DL= 12.9 <br />MDL <br />0.887 <br />2.56 <br />3.08 <br />5.29 <br />2.96 <br />5.40 <br />3.93 <br />DL= 4.68 <br />DL= 4.51 <br />DL= 7.69 <br />DL= 4.00 <br />DL= 6.86 <br />DL= 8.50 <br />DL= 8.50 <br />DL= 11.2 <br />DL= 12.9 <br />DL= 12.7 <br />Conc. (pg/L) <br />DL= 2.99 <br />Total HxCDF <br />Total HpCDF <br />DL= 7.69 <br />DL= 16.0 <br />DL= 4.00 <br />DL= 6.86 <br />DL= 5.53 <br />DL= 6.99 <br />DL= 4.53 <br />DL= 6.79 <br />Total TCDD <br />Total PeCDD <br />Total HxCDD <br />Total HpCDD <br />Total TCDF <br />Total PeCDF <br />234678-HxCDF <br />123789-HxCDF <br />1234678-HpCDF <br />1234789-HpCDF <br />OCDF <br />Totals <br />123678-HxCDD <br />123789-HxCDD <br />12378-PeCDF <br />23478-PeCDF <br />123478-HxCDF <br />123678-HxCDF <br />Analyte <br />2,3,7,8-TCDD <br />12378-PeCDD <br />123478-HxCDD <br />5.15 <br />8.50 <br />0.733 <br />DL= 2.99 <br />DL= 4.68 <br />DL= 4.31 <br />DL= 4.51 <br />DL= 4.32 <br />Date Received:Ceres Sample ID:12701-001 <br />13.1 <br />37Cl4-2378-TCDD <br />13C-123678-HxCDF <br />EPA Method 1613B <br />66.2 <br />35.1 <br />47.7 <br />11:30 <br />QC Batch #: <br />3/12/2019 <br />31.9 <br />34.4 <br />69.7 <br />38.3 <br />28.7 <br />1964 <br />46.5 <br />25.6 <br />27.4 <br />34.5 <br />B13-Water <br />Labeled Standards % R <br />Matrix: <br />Sample Size: <br />Qual.Conc. (pg/L) <br />Client Sample ID: <br />Date Collected: <br />Time Collected:NA <br />Date Extracted: <br />Q-225 Analysis: <br />Aqueous 4/4/2019 <br />4/1/2019 <br />ZB-5MS Analysis: <br />3/20/2019 <br />Qualifiers <br />25-16413C-2378-TCDD <br />13C-12378-PeCDD <br />13C-123478-HxCDD <br />13C-123678-HxCDD <br />LCL-UCL (a) <br />38.9 <br />41.5 <br />1234678-HpCDD <br />OCDD <br />2,3,7,8-TCDF <br />13C-1234678-HpCDF <br />13C-OCDD <br />13C-2378-TCDF <br />13C-234678-HxCDF <br />13C-123789-HxCDF <br />13C-12378-PeCDF <br />13C-123478-HxCDF <br />23-140 <br />17-157 <br />13C-1234678-HpCDD <br />13C-23478-PeCDF <br />25-181 <br />32-141 <br />28-130 <br />24-169 <br />33.1 <br />26-152 <br />26-123 <br />24-185 <br />21-178 <br />13C-1234789-HpCDF <br />28-136 <br />29-147 <br />28-143 <br />26-138 <br />(b) - TEQ based on (2005) World Health Organization (WHO) Toxic <br />32.0 <br />Total Toxic Equivalency (TEQ min.) (b):0.0 <br />DL - Signifies Non-Detect (ND) at sample specific detection limit. <br />EMPC - Estimated Maximum Possible Concentration due to ion abundance <br /> ratio failure. <br />(a) - Lower control limit - Upper control limit <br />pg/L <br /> Equivalent Factors. <br />Project ID:14-3002 <br />0.941 <br />35-197 <br />CRS <br />Page 6 of 29