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g <br />Analyst: JMH Reviewed by: BS <br />0.425 <br />0.0886 <br />0.412 <br />0.422 <br />0.518 <br />35-197 <br />CRS <br />1.01 <br />28-136 <br />24-169 <br />0.533 <br />0.319 <br />DL= 0.345 <br />DL= 0.388 <br />1.55 <br />0.315 <br />0.409 <br />0.655 <br />Total Toxic Equivalency (TEQ min.) (b):4.93 <br />DL - Signifies Non-Detect (ND) at sample specific detection limit. <br />EMPC - Estimated Maximum Possible Concentration due to ion abundance <br /> ratio failure. <br />(a) - Lower control limit - Upper control limit <br />(b) - TEQ based on (2005) World Health Organization (WHO) Toxic <br /> Equivalent Factors. <br />pg/g <br />Total TCDF <br />29-147 <br />28-143 <br />26-138 <br />21-178 <br />26-152 <br />13C-1234678-HpCDD <br />26-123 <br />Qualifiers <br />25-164 <br />25-181 <br />32-141 <br />28-130 <br />24-185 <br />LCL-UCL (a) <br />84.1 <br />86.0 <br />23-140 <br />17-157 <br />13C-12378-PeCDF <br />Labeled Standards % R <br />13C-2378-TCDD <br />81.7 <br />13C-123478-HxCDF <br />13C-12378-PeCDD <br />13C-123478-HxCDD <br />13C-123678-HxCDD <br />13C-23478-PeCDF <br />13C-OCDD <br />13C-2378-TCDF <br />13C-1234789-HpCDF <br />37Cl4-2378-TCDD <br />13C-123678-HxCDF <br />13C-234678-HxCDF <br />13C-123789-HxCDF <br />13C-1234678-HpCDF <br />123678-HxCDD <br />123789-HxCDD <br />234678-HxCDF <br />123789-HxCDF <br />DL= 0.326 <br />DL= 0.336 <br />DL= 0.355 <br />DL= 0.391 <br />12378-PeCDD <br />123478-HxCDD <br />23478-PeCDF <br />123478-HxCDF <br />123678-HxCDF <br />3.37 <br />3/29/2019 <br />ZB-5MS Analysis: <br />Date Received: <br />Date Collected: <br />QC Batch #: <br />14-3002Project ID:Ceres Sample ID: <br />Date Extracted: <br />Q-225 Analysis: <br />Soil 4/2/2019 <br />2,3,7,8-TCDD 94.8 <br />3/15/2019 <br />10:15 AMTime Collected:% Solids:97.1 <br />Conc. (pg/g) <br />EPA Method 1613B <br />3/20/2019 <br />Analyte <br />Client Sample ID: <br />4/3/2019 <br />B40-10 <br />61.7 <br />97.1 <br />85.3 <br />83.1 <br />87.2 <br />83.7 <br />94.8 <br />12701-016 <br />1965 <br />Matrix: <br />Sample Size: <br />81.0 <br />92.1 <br />80.0 <br />71.3 <br />94.7 <br />Qual. <br />1234678-HpCDD <br />OCDD <br />2,3,7,8-TCDF <br />12378-PeCDF <br />1234678-HpCDF <br />1234789-HpCDF <br />OCDF <br />Totals <br />Total TCDD <br />Total PeCDD <br />Total HxCDD <br />Total HpCDD <br />Total PeCDF <br />Total HxCDF <br />Total HpCDF <br />7.94 <br />7.60 <br />95.2 <br />241 <br />10.3 <br />4.37 <br />2.52 <br />DL= 0.536 <br />DL= 2.10 <br />Conc. (pg/g) <br />5.51 <br />7.66 <br />60.6 <br />161 <br />101 <br />28.4 <br />3.49 <br />2.52 <br />MDL <br />0.172 <br />0.327 <br />0.327 <br />0.279 <br />0.378 <br />0.461 <br />EMPC <br />J <br />2.48 <br />2.48 <br />2.48 <br />2.48 <br />2.48 <br />RL <br />0.496 <br />2.48 <br />2.48 <br />10.38 <br />2.48 <br />2.48 <br />2.48 <br />2.48 <br />4.96 <br />4.96 <br />0.496 <br />2.48 <br />2.48 <br />Page 25 of 29