COMPLIANCE INFO_10/7/24 SITE CHARACTERIAZTION RPT

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Details ReportSection.FieldDetails Sample Name DP-15-10 Sampling Site Enthalpy ID 0824-1274-001-1 Prep Batch EU18061 Tare Weight (g)0.94 Matrix solids Analyst jemunoz Wet Weight (g)3.15 Sampling Date 2024-08-20 14:57 Instrument Gandalf Dry Weight (g)2.87 Received Date 2024-08-28 Sample Vol mL N/A Extr. Mass (g)9.88 Prep Date 2024-08-30 16:00 Extract Vol mL 0.02 Net Weight (g)2.21 AnalysisDate 2024-09-23 12:19 Split Factor N/A Dry Weight (g)2.87 SampleType Sample Method Code EU-045-90S % Solids 87.3% Bottle ID -Dry Wt. Equiv (g)8.63 Compound CAS Injection File Name Sample Concentration pg/g LOQ pg/g EDL pg/g Recovery Limits Recovery Flags TCDD 2378-TCDD (S)1746-01-6 G21092458B 0.839 0.579 0.750 PeCDD 12378-PeCDD (S)40321-76-4 G21092458B 3.26 2.90 0.782 HxCDD 123478-HxCDD (S)39227-28-6 G21092458B 1.65 2.90 0.833 J HxCDD 123678-HxCDD (S)57653-85-7 G21092458B 4.65 2.90 0.808 HxCDD 123789-HxCDD (S)19408-74-3 G21092458B 2.17 2.90 0.977 J HpCDD 1234678-HpCDD (S)35822-46-9 G21092458B 13.2 2.90 1.06 OCDD OCDD (S)3268-87-9 G21092458B 32.8 5.79 3.49 TCDF 2378-TCDF (S)51207-31-9 G21092458B 34.5 0.579 1.11 PeCDF 12378-PeCDF (S)57117-41-6 G21092458B 12.6 2.90 0.913 PeCDF 23478-PeCDF (S)57117-31-4 G21092458B 45.6 2.90 0.993 HxCDF 123478-HxCDF (S)70648-26-9 G21092458B 16.1 2.90 1.17 HxCDF 123678-HxCDF (S)57117-44-9 G21092458B 15.0 2.90 1.20 HxCDF 234678-HxCDF (S)60851-34-5 G21092458B 22.9 2.90 1.19 HxCDF 123789-HxCDF (S)72918-21-9 G21092458B 1.31 2.90 1.85 J-EMPC HpCDF 1234678-HpCDF (S)67562-39-4 G21092458B 42.4 2.90 1.27 HpCDF 1234789-HpCDF (S)55673-89-7 G21092458B ND 2.90 1.82 U OCDF OCDF (S)39001-02-0 G21092458B ND 5.79 0.994 U ES 13C-2378-TCDD (ES)76523-40-5 G21092458B 1.92 40-135%88.2% ES 13C-12378-PeCDD (ES)109719-79-1 G21092458B 2.99 40-135%92.5% ES 13C-123478-HxCDD (ES)109719-80-4 G21092458B 1.58 40-135%74.7% ES 13C-123678-HxCDD (ES)109719-81-5 G21092458B 1.46 40-135%102% ES 13C-123789-HxCDD (ES)109719-82-6 G21092458B 1.48 40-135%92.9% ES 13C-1234678-HpCDD (ES)109719-83-7 G21092458B 2.11 40-135%124% ES 13C-OCDD (ES)114423-97-1 G21092458B 1.59 40-135%112% ES 13C-2378-TCDF (ES)89059-46-1 G21092458B 1.72 40-135%94.6% ES 13C-12378-PeCDF (ES)109719-77-9 G21092458B 2.30 40-135%104% ES 13C-23478-PeCDF (ES)116843-02-8 G21092458B 2.37 40-135%98.7% ES 13C-123478-HxCDF (ES)114423-98-2 G21092458B 2.00 40-135%84.0% ES 13C-123678-HxCDF (ES)116843-03-9 G21092458B 1.76 40-135%95.2% ES 13C-234678-HxCDF (ES)116843-05-1 G21092458B 1.84 40-135%86.6% ES 13C-123789-HxCDF (ES)116843-04-0 G21092458B 2.21 40-135%107% ES 13C-1234678-HpCDF (ES)109719-84-8 G21092458B 2.50 40-135%117% ES 13C-1234789-HpCDF (ES)109719-94-0 G21092458B 2.95 40-135%121% ES 13C-OCDF (ES)109719-78-0 G21092458B 1.27 40-135%117% CS 37Cl-2378-TCDD (CS)G21092458B 0.646 20-150%112% CS 13C-12347-PeCDD (CS)G21092458B 3.24 20-150%99.9% CS 13C-12346-PeCDF (CS)G21092458B 2.38 20-150%118% CS 13C-123469-HxCDF (CS)G21092458B 2.14 20-150%121% CS 13C-1234689-HpCDF (CS)G21092458B 2.75 20-150%144% AS 13C-1368-TCDD (AS)G21092458B 1.79 20-150%110% AS 13C-1368-TCDF (AS)G21092458B 1.43 20-150%116% TCDD Group Total 41903-57-5 54.3 0.750 PeCDD Group Total 36088-22-9 50.4 0.782 HxCDD Group Total 34465-46-8 61.0 0.873 HpCDD Group Total 37871-00-4 22.8 1.06 OCDD Group Total 32.8 3.49 TCDF Group Total 55722-27-5 772 1.11 PeCDF Group Total 30402-15-4 373 0.953 HxCDF Group Total 55684-94-1 163 1.36 HpCDF Group Total 38998-75-3 44.4 1.55 OCDF Group Total ND 0.994 TEQ ITEQ (ND=0; EMPC=0)36.2 ITEQ (ND=1/2EDL;EMPC=1/2EDL)36.3 ITEQ (ND=EDL EMPC=EDL)36.4 ITEQ (ND=0; EMPC=EMPC)36.3 ITEQ (ND=1/2EDL; EMPC=EMPC)36.4 ITEQ (ND=EDL; EMPC=EMPC)36.4 WTEQ (ND=0; EMPC=0)28.4 WTEQ (ND=1/2EDL;EMPC=1/2EDL)28.5 WTEQ (ND=EDL EMPC=EDL)28.6 Enthalpy Analytical Job No.: 0824-1274-1 EPA Method 8290A Solid Enthalpy Analytical, Orange, CA EO-514512 EU 0824-1274 Page 10 of 20 83 of 95