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1534 Willow Pass Road,Pittsburg,CA 94565-1701 M c C a m p b e I l Analytical, Inc. Toll Free Telephone:(877)252-9262/Fax:(925)252-9269 "When Quality Counts" http://www.mccarnpbell.com/E-mail:main@mccampbell.com Quality Control Report Client: ICES WorkOrder: 241 OL96 Date Prepared: 10/29/2024 BatchID: 304930 Date Analyzed: 11/04/2024 Extraction Method: SW3550B Instrument: GC20 Analytical Method: SW8081B Matrix: Soil Unit: mg/kg Project: ICES 9315;Kautz Property Sample ID: MB/LCS/LCSD-304930 QC Summary Report for SW8081B Analyte LCS LCSD SPK LCS LCSD LCS/LCSD RPD RPD Result Result Val %REC %REC Limits Limit Aldrin 0.044 0.044 0.050 87 88 70-130 0.266 20 a-BHC 0.046 0.046 0.050 93 92 70-130 0.191 20 b-BHC 0.043 0.043 0.050 87 86 70-130 0.430 20 d-BHC 0.040 0.040 0.050 81 80 70-130 1.74 20 g-BHC 0.047 0.047 0.050 94 94 70-130 0.390 20 a-Chlordane 0.046 0.045 0.050 91 90 70-130 1.11 20 g-Chlordane 0.041 0.041 0.050 83 82 70-130 1.09 20 p,p-DDD 0.058 0.056 0.050 116 111 70-130 3.90 20 p,p-DDE 0.055 0.054 0.050 110 108 70-130 2.34 20 p,p-DDT 0.048 0.044 0.050 95 88 70-130 7.82 20 Dieldrin 0.049 0.048 0.050 97 96 70-130 1.31 20 Endosulfan 1 0.045 0.044 0.050 89 89 70-130 0.816 20 Endosulfan 11 0.045 0.044 0.050 90 88 70-130 2.75 20 Endosulfan sulfate 0.046 0.044 0.050 92 88 70-130 4.02 20 Endrin 0.077 0.074 0.050 154,F2 149,F2 70-130 3.45 20 Endrin aldehyde 0.043 0.042 0.050 87 84 70-130 3.24 20 Endrin ketone 0.041 0.039 0.050 82 78 70-130 5.41 20 Heptachlor 0.049 0.048 0.050 98 96 70-130 1.81 20 Heptachlor epoxide 0.046 0.046 0.050 92 91 70-130 0.420 20 Hexachlorobenzene 0.043 0.043 0.050 86 85 70-130 0.450 20 Hexachlorocyclopentadiene 0.035 0.033 0.050 70 67 50-130 4.76 20 Methoxychlor 0.051 0.046 0.050 101 93 70-130 8.70 20 Surrogate Recovery Decachlorobiphenyl 0.055 0.049 0.050 110 99 70-130 11.2 20 CA ELAP 1644•NELAP 4033ORELAP Page 12 of 17