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Active Groundwater Sampling Standard Operating Procedure <br /> SWE-FSOP-401;Revision 1 Ahtna Southwest Environmental Operations <br /> If other sample analyses are required,fill the other sample containers after filling the VOC/or GRO sample <br /> vials. Fill each bottle to the base of the bottleneck. Care will be taken to avoid aerating the sample and <br /> not overfill bottles containing preservatives. All samples shall be appropriately preserved as described in <br /> the project plans. Each sample container to be submitted for analysis will be appropriately labeled per <br /> SWE-FSOP-002 (Field Sample Management). <br /> When there is an insufficient of grounwater(limited recharge)the samples should be collected in an order <br /> of analysis specified by the FTL in coordination with the PL to meet project objectives. Altenately, fill <br /> containers in the following order. <br /> 1. Purgeable organic carbons 10. Phenols <br /> 2. Purgeable organic halogens 11. Cyanide <br /> 3. Total organic halogens 12. Anions <br /> 4. TOC 13. Ammonia <br /> 5. Base neutrals/acid extractables 14. Preserved inorganics <br /> 6. Total petroleum hydrocarbons 15. Radionuclides <br /> 7. PCBs/pesticides 16. Non-preserved inorganics <br /> 8. Total metals 17. Bacteria. <br /> 9. Dissolved metals <br /> A clean 0.45-micron filter is attached to tubing connected to the positive-displacement pump and poured <br /> directly into the sample container to collect filtered samples. Samples collected without pumps can be <br /> poured into an unpreserved sample container and then pumped through the filter using a peristaltic <br /> pump. Hand pumps are commercially available as an alternative. Larger pore size filters can be used in <br /> series with the 0.45-micron filter to reduce suspended solids from the water. <br /> 4.8 Document Control <br /> Sampling field forms should be completed in their entirety. If an entry is not applicable, indicate "n/a" <br /> (not applicable) or line out the entry. <br /> After a task or project,all field documentation, including the field logbook,field datasheets,and electronic <br /> data, shall be scanned and placed on the server in the appropriate folder. All original documents shall be <br /> submitted to the PL and kept in the project file. See FSOP-001 (Field Documentation). <br /> 5.0 Quality Assurance/Quality Control <br /> Conduct the 3-Phases of Quality Control method described in the project work plans. <br /> The values of the water quality parameter measurements and water depths must be compared to the <br /> previous event measurements to assess the reasonableness of the new data. If a water quality parameter <br /> measurement is inconsistent with the past measurement, then an instrument check of a calibration <br /> standard for the suspect parameter should be performed. If the calibration is out of specifications, the <br /> instrument should be repaired or replaced,the suspect parameter measurement should be evaluated for <br /> Page 13 of 14 <br />