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Pace Analytical Services,LLC <br /> (�Ia'ucnba.Analytical® 1700 Elm Street-Suite 200 <br /> www.pacelabs.com Minneapolis,MN 55414 <br /> (612)607-1700 <br /> QUALITY CONTROL DATA <br /> Project: 7036 French Camp CA-Lathrop In-Revised Report <br /> Pace Project No.: 10508446 <br /> QC Batch: 659949 Analysis Method: EPA 8015 Modified <br /> QC Batch Method: EPA 3550 Sonication Analysis Description: 8015 Solid GCSV <br /> Associated Lab Samples: 10508446001,10508446002, 10508446003, 10508446004, 10508446005, 10508446007, 10508446008, <br /> 10508446009, 10508446010, 10508446011, 10508446012, 10508446013, 10508446014, 10508446015, <br /> 10508446016, 10508446017, 10508446018 <br /> METHOD BLANK: 3541948 Matrix: Solid <br /> Associated Lab Samples: 10508446001, 10508446002, 10508446003, 10508446004, 10508446005, 10508446007, 10508446008, <br /> 10508446009, 10508446010, 10508446011, 10508446012, 10508446013, 10508446014, 10508446015, <br /> 10508446016, 10508446017, 10508446018 <br /> Blank Reporting <br /> Parameter Units Result Limit Analyzed Qualifiers <br /> Motor Oil Range(C24-C36) mg/kg ND 10.0 02/15/20 12:11 N2 <br /> TPH-DRO(C10-C28) mg/kg ND 10.0 02/15/20 12:11 <br /> n-Triacontane(S) %. 87 30-144 02/15/20 12:11 <br /> o-Terphenyl(S) %. 78 30-146 02/15/20 12:11 <br /> LABORATORY CONTROL SAMPLE: 3541949 <br /> Spike LCS LCS %Rec <br /> Parameter Units Conc. Result %Rec Limits Qualifiers <br /> Motor Oil Range(C24-C36) mg/kg 50 46.0 92 75-125 N2 <br /> TPH-DRO(C10-C28) mg/kg 50 43.1 86 66-125 <br /> n-Triacontane(S) %. 90 30-144 <br /> o-Terphenyl(S) %. 89 30-146 <br /> MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 3541950 3541951 <br /> MS MSD <br /> 10508446001 Spike Spike MS MSD MS MSD %Rec Max <br /> Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD RPD Qual <br /> Motor Oil Range(C24-C36) mg/kg 659 48.8 49.6 737 665 161 12 54-146 10 30 M6,N2 <br /> TPH-DRO(C10-C28) mg/kg 9110 48.8 49.6 9900 8850 1630 -513 39-135 11 30 M6 <br /> n-Triacontane(S) %. 0 0 30-144 S4 <br /> o-Terphenyl(S) %. 0 0 30-146 S4 <br /> Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. <br /> REPORT OF LABORATORY ANALYSIS <br /> This report shall not be reproduced,except in full, <br /> Date:03/20/2020 02:52 PM without the written consent of Pace Analytical Services,LLC. Page 14 of 39 <br />