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QC Sample Results Client: Patriot Environmental Services Job ID: 720-93886-1 Project/Site: UPRR-French Camp ------ - - ----- --- -------------------------- ------ -- - - -- - --- — -- --- Method: 8260B -Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: MB 440-556994/4 Client Sample ID: Method Blank Matrix: Solid Prep Type: Total/NA Analysis Batch: 556994 MB MB Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Toluene-d8(Surr) 97 79-123 07/11/19 08:47 1 Lab Sample ID: LCS 440-556994/5 Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Total/NA Analysis Batch: 556994 Spike LCS LCS %Rec. Analyte Added Result Qualifier Unit D %Rec Limits Methylene Chloride 20.0 17.2 ug/Kg 86 55-135 n-Butylbenzene 20.0 19.1 ug/Kg 95 70-130 LCS LCS Surrogate %Recovery Qualifier Limits 4-Bromofluorobenzene(Surr) 85 79-120 Dibromonuoromethane(Surr) 99 60-120 Toluene-d8(Surr) 94 79-123 Method: 8270C - Semivolatile Organic Compounds (GC/MS) Lab Sample ID: MB 440-556805/1-A Client Sample ID: Method Blank Matrix: Solid Prep Type: Total/NA Analysis Batch: 556835 Prep Batch: 556805 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,2,4-Trichlorobenzene ND 250 100 ug/Kg 6-7/10/19-07 25 T7—/10/1913 10 1 1,2-Dichlorobenzene ND 250 52 ug/Kg 07/10/19 07:25 07/10/19 13:10 1 1,2-Diphenylhydrazine(as ND 250 52 ug/Kg 07/10/19 07:25 07/10/19 13:10 1 Azobenzene) 1,3-Dichlorobenzene ND 250 100 ug/Kg 07/10/1907:25 07/10/1913:10 1 1,4-Dichlorobenzene ND 250 100 ug/Kg 07/10/19 07:25 07/10/19 13:10 1 2,4,5-Trichlorophenol ND 500 200 ug/Kg 07/10/19 07:25 07/10/19 13:10 1 2,4,6-Trichlorophenol ND 500 160 ug/Kg 07/10/19 07:25 07/10/19 13:10 1 2,4-Dichlorophenol ND 250 50 ug/Kg 07/10/19 07:25 07/10/19 13:10 1 2,4-Dimethylphenol ND 250 98 ug/Kg 07/10/19 07:25 07/10/19 13:10 1 2,4-Dinitrophenol ND 1000 750 ug/Kg 07/10/19 07:25 07/10/19 13:10 1 2,4-Dinitrotoluene ND 250 60 ug/Kg 07/10/19 07:25 07/10/19 13:10 1 2,6-Dinitrotoluene ND 250 71 ug/Kg 07/10/19 07:25 07/10/19 13:10 1 2-Chloronaphthalene ND 250 50 ug/Kg 07/10/19 07:25 07/10/19 13:10 1 2-Chlorophenol ND 250 52 ug/Kg 07/10/19 07:25 07/10/19 13:10 1 2-Methylnaphthalene ND 250 52 ug/Kg 07/10/19 07:25 07/10/19 13:10 1 2-Methylphenol ND 250 60 ug/Kg 07/10/19 07:25 07/10/19 13:10 1 2-Nitroaniline ND 250 170 ug/Kg 07/10/19 07:25 07/10/19 13:10 1 2-Nitrophenol ND 250 100 ug/Kg 07/10/19 07:25 07/10/19 13:10 1 3,3'-Dichlorobenzidine ND 500 110 ug/Kg 07/10/19 07:25 07/10/19 13:10 1 3-Nitroaniline ND 250 100 ug/Kg 07/10/19 07:25 07/10/19 13:10 1 4,6-Dinitro-2-methylphenol ND 420 100 ug/Kg 07/10/19 07:25 07/10/19 13:10 1 4-Bromophenyl phenyl ether ND 250 56 ug/Kg 07/10/19 07:25 07/10/19 13:10 1 4-Chloro-3-methylphenol ND 400 150 ug/Kg 07/10/19 07:25 07/10/19 13:10 1 4-Chloroaniline ND 500 150 ug/Kg 07/10/19 07:25 07/10/19 13:10 1 4-Chlorophenyl phenyl ether ND 500 200 ug/Kg 07/10/19 07:25 07/10/19 13:10 1 3-Methylphenol+4-Methylphenol ND 250 100 ug/Kg 07/10/19 07:25 07/10/19 13:10 1 Eurofins TestAmerica, Pleasanton Page 21 of 37 7/15/2019