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QC Sample Results Client: Patriot Environmental Services Job ID: 720-93886-1 Project/Site: UPRR-French Camp Method: 60108 - Metals (ICP) Lab Sample ID: MB 440-557085/1-A "5 Client Sample ID: Method Blank Matrix: Solid Prep Type: Total/NA Analysis Batch: 557455 Prep Batch: 557085 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Antimony ND 10 5.o mg/Kg 07/11/1914:14 07/12/1916:01 5 Arsenic ND 3.0 1.5 mg/Kg 07/11/1914:14 07/12/1916:01 5 Barium ND 1.5 0.75 mg/Kg 07/11/1914:14 07/12/1916:01 5 Beryllium ND 0.50 0.25 mg/Kg 07/11/1914:14 07/12/1916:01 5 Cadmium ND 0.50 0.25 mg/Kg 07/11/1914:14 07/12/1916:01 5 Chromium ND 1.0 0.50 mg/Kg 07/11/1914:14 07/12/1916:01 5 Cobalt ND 1.0 0.50 mg/Kg 07/11/1914:14 07/12/1916:01 5 Copper ND 2.0 1.1 mg/Kg 07/11/1914:14 07/12/1916:01 5 Lead ND 2.0 1.0 mg/Kg 07/11/1914:14 07/12/1916:01 5 Molybdenum ND 2.0 1.0 mg/Kg 07/11/1914:14 07/12/1916:01 5 Nickel ND 2.0 1.0 mg/Kg 07/11/1914:14 07/12/1916:01 5 Selenium ND 3.0 1.7 mg/Kg 07/11/1914:14 07/12/1916:01 5 Thallium ND 10 5.0 mg/Kg 07/11/1914:14 07/12/1916:01 5 Vanadium ND 1.0 0.50 mg/Kg 07/11/1914:14 07/12/1916:01 5 Zinc ND 5.0 2.5 mg/Kg 07/11/1914:14 07/12/1916:01 5 Silver ND 1.5 0.89 mg/Kg 07/11/1914:14 07/12/1916:01 5 Lab Sample ID: LCS 440-557085/2-A ^5 Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Total/NA Analysis Batch: 557455 Prep Batch: 557085 Spike LCS LCS %Rec. Analyte Added Result Qualifier Unit D %Rec Limits Antimony 49.5 52.9 mg/Kg 107 80-120 Arsenic 49.5 52.2 mg/Kg 106 80-120 Barium 49.5 52.0 mg/Kg 105 80-120 Beryllium 49.5 51.2 mg/Kg 103 80-120 Cadmium 49.5 51.5 mg/Kg 104 80-120 Chromium 49.5 52.1 mg/Kg 105 80-120 Cobalt 49.5 52.3 mg/Kg 106 80-120 Copper 49.5 53.8 mg/Kg 109 80-120 Lead 49.5 53.0 mg/Kg 107 80-120 Molybdenum 49.5 56.7 mg/Kg 115 80-120 Nickel 49.5 53.1 mg/Kg 107 80-120 Selenium 49.5 49.4 mg/Kg 100 80-120 Thallium 49.5 48.5 mg/Kg 98 80-120 Vanadium 49.5 51.8 mg/Kg 105 80-120 Zinc 49.5 52.0 mg/Kg 105 80-120 Silver 24.8 25.8 mg/Kg 104 80-120 Lab Sample ID: 720-93886-1 MS Client Sample ID: 001 Matrix: Solid Prep Type: Total/NA Analysis Batch: 557455 Prep Batch: 557085 Sample Sample Spike MS MS %Rec. Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits Antimony ND 49.5 40.6 mg/Kg 82 75-125 Arsenic 3.7 49.5 58.0 mg/Kg 110 75-125 Barium 77 F1 F2 49.5 169 F1 mg/Kg 186 75-125 Beryllium ND 49.5 52.6 mg/Kg 106 75-125 Cadmium ND 49.5 51.5 mg/Kg 104 75-125 Eurofins TestAmerica, Pleasanton Page 26 of 37 7/15/2019