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Surrogate Summary <br /> Client: Union Pacific Railroad TestAmerica Job ID: 720-74752-1 <br /> Project/Site: UPRR-Stockton <br /> Method: 8270C -Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS) <br /> Matrix:Solid Prep Type:Total/NA <br /> Percent Surrogate Recovery(Acceptance Limits) <br /> NBZ FBP TPH 2FP PHL TBP <br /> Lab Sample ID Client Sample ID (21-98) (30-112) (59-134) (28-98) (23-101) (37-114) <br /> 720-74752-1 MR505 UPRRST160927 ox ox ox ox ox ox <br /> LCS 720-210923/2-A Lab Control Sample 82 90 106 81 82 95 <br /> MB 720-210923/1-A Method Blank 80 94 111 76 72 82 <br /> Surrogate Legend <br /> NBZ=Nitrobenzene-d5 <br /> FBP=2-Fluorobiphenyl <br /> TPH=Terphenyl-d14 <br /> 2FP=2-Fluorophenol <br /> PHL=Phenol-d5 <br /> TBP=2,4,6-Tribromophenol <br /> Method: 8015B -Diesel Range Organics (DRO) (GC) <br /> Matrix:Solid Prep Type:Total/NA <br /> Percent Surrogate Recovery(Acceptance Limits) <br /> PTP1 <br /> Lab Sample ID Client Sample ID (40-130) <br /> 720-74752-1 MR505 UPRRST160927 0 X D <br /> LCS 720-210810/2-A Lab Control Sample 116 <br /> MB 720-210810/1-A Method Blank 98 <br /> Surrogate Legend <br /> PTP=p-Terphenyl <br /> TestAmerica Pleasanton <br /> Page 9 of 27 10/17/2016 <br />