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QC Sample Results <br /> Client: Union Pacific Railroad TestAmerica Job ID: 720-74752-1 <br /> Project/Site: UPRR-Stockton <br /> ......_...... <br /> Method: 6010B -Metals (ICP) (Continued) <br /> Lab Sample ID:MB 720-210351/1-A Client Sample ID:Method Blank <br /> Matrix:Solid Prep Type:Total/NA <br /> Analysis Batch:210649 Prep Batch:210351 <br /> MB MB <br /> Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac <br /> Cadmium ND 0.13 mg/Kg 09/30/16 12:36 10/04/16 20:03 1 <br /> Chromium ND 0.50 mg/Kg 09/30/16 12:36 10/04/16 20:03 1 <br /> Cobalt ND 0.20 mg/Kg 09/30/16 12:36 10/04/16 20:03 1 <br /> Copper ND 1.5 mg/Kg 09/30/1612:36 10/04/1620:03 1 <br /> Lead ND 0.50 mg/Kg 09/30/16 12:36 10/04/16 20:03 1 <br /> Molybdenum ND 0.50 mg/Kg 09/30/16 12:36 10/04/16 20:03 1 <br /> Nickel ND 0.50 mg/Kg 09/30/16 12.36 10/04/16 20:03 1 <br /> Selenium ND 1.0 mg/Kg 09/30/1612:36 10/04/1620:03 1 <br /> Silver ND 0.25 mg/Kg 09/30/1612:36 10/04/1620:03 1 <br /> Thallium ND 0.50 mg/Kg 09/30/16 12.36 10/04/16 20:03 1 <br /> Vanadium ND 0.50 mg/Kg 09/30/16 12:36 10/04/16 20:03 1 <br /> Zinc ND 1.5 mg/Kg 09/30/16 12:36 10/04/16 20:03 1 <br /> Lab Sample ID:LCS 720-210351/2-A Client Sample ID: Lab Control Sample <br /> Matrix:Solid Prep Type:Total/NA <br /> Analysis Batch:210649 Prep Batch:210351 <br /> Spike LCS LCS %Rec. <br /> Analyte Added Result Qualifier Unit D %Rec Limits <br /> Antimony 50.0 47.0 mg/Kg 94 80-120 <br /> Arsenic 50.0 47.4 mg/Kg 95 80-120 <br /> Barium 50.0 49.9 mg/Kg 100 80-120 <br /> Beryllium 50.0 49.9 mg/Kg 100 80-120 <br /> Cadmium 50.0 48.1 mg/Kg 96 80-120 <br /> Chromium 50.0 49.4 mg/Kg 99 80-120 <br /> Cobalt 50.0 49.0 mg/Kg 98 80-120 <br /> Copper 50.0 49.0 mg/Kg 98 80-120 <br /> Lead 50.0 48.8 mg/Kg 98 80-120 <br /> Molybdenum 50.0 48.9 mg/Kg 98 80.120 <br /> Nickel 50.0 49.0 mg/Kg 98 80-120 <br /> Selenium 50.0 46.4 mg/Kg 93 80-120 <br /> Silver 25.0 24.1 mg/Kg 96 80-120 <br /> Thallium 50.0 49.8 mg/Kg 100 80-120 <br /> Vanadium 50.0 48.6 mg/Kg 97 80-120 <br /> Zinc 50.0 48.0 mg/Kg 96 80-120 <br /> Lab Sample ID:LCSSRM 720-210351/3-A Client Sample ID:Lab Control Sample <br /> Matrix:Solid Prep Type:Total/NA <br /> Analysis Batch:210649 Prep Batch:210351 <br /> Spike LCSSRM LCSSRM %Rec. <br /> Analyte Added Result Qualifier Unit D %Rec Limits <br /> Antimony 74.6 34.4 mg/Kg 46 11_101 <br /> Arsenic 45.5 39.8 mg/Kg 87 69-119 <br /> Barium 579 526 mg/Kg 91 61-117 <br /> Beryllium 155 133 mg/Kg 86 56-102 <br /> Cadmium 201 177 mg/Kg 88 67-118 <br /> Chromium 106 93.8 mg/Kg 88 67-121 <br /> Cobalt 247 219 mg/Kg 89 64-133 <br /> Copper 130 121 mg/Kg 93 68-126 <br /> Lead 302 256 mg/Kg 85 62-113 <br /> TestAmerica Pleasanton <br /> Page 14 of 27 10/17/2016 <br />