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Case Narrative <br /> Client: United Pumping Service TestAmerica Job ID:440-212315-2 <br /> Project/Site: UPRR-Stockton MR-572 Onespot <br /> - - --— <br /> Job ID: 440-212315-1 (Continued) <br /> Laboratory: TestAmerica Irvine (Continued) <br /> limits. , <br /> Method(s)6010B:The post digestion spike% recovery for Barium associated with batch 440-481158 was outside of control limits. <br /> Method(s)6010B:The method blank for preparation batch 440-479766 and analytical batch 440-481158 contained Chromium above the <br /> reporting limit(RL). Associated sample(s)were not re-extracted and/or re-analyzed because results were greater than 1 OX the value <br /> found in the method blank. <br /> Method(s)7471A:The matrix spike/matrix spike duplicate(MS/MSD)recoveries for preparation batch 440-479337 and analytical batch <br /> 440-479582 were outside control limits. The associated laboratory control sample(LCS)recovery was within acceptance limits. <br /> No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page. <br /> Subcontract non-Sister <br /> No analytical or quality issues were noted, other than those described in the Definitions/Glossary page. <br /> Organic Prep <br /> Method(s)3546: Due to the matrix,the following sample could not be concentrated to the final method required volume: UPSTKMR-572 <br /> (440-212315-1). The reporting limits(RLs)are elevated proportionately.440-479159 3546 8015—DRO <br /> No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page. <br /> VOA Prep <br /> No analytical or quality issues were noted, other than those described in the Definitions/Glossary page. <br /> Job ID: 440-212315-2 <br /> Laboratory: TestAmerica Irvine <br /> Narrative <br /> Job Narrative <br /> 440-212315-2 <br /> Comments <br /> Amended to add STLCfFCLP Lead. <br /> Receipt <br /> The sample was received on 5/29/2018 2:50 PM;the sample arrived in good condition, properly preserved and,where required, on ice. <br /> The temperature of the cooler at receipt was 3.4°C. <br /> Metals <br /> No analytical or quality issues were noted, other than those described in the Definitions/Glossary page. <br /> Organic Prep <br /> No analytical or quality issues were noted, other than those described in the Definitions/Glossary page. <br /> TestAmerica Irvine <br /> Page 5 of 32 6/19/2018 <br />