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QC Sample Results <br /> Client: United Pumping Service TestAmerica Job ID:440-212315-2 <br /> Project/Site: UPRR-Stockton MR-572 Onespot <br /> Method: 6010B - Metals (ICP) (Continued) <br /> Lab Sample ID: 440-212516-A-1-D MSD "5 Client Sample ID: Matrix Spike Duplicate <br /> Matrix: Solid Prep Type: Total/NA <br /> Analysis Batch: 481158 Prep Batch: 479766 <br /> Sample Sample Spike MSD MSD %Rec. RPD <br /> Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits RPD Limit <br /> Cadmium ND 49.3 44.4 mg/Kg 90 75-125 3 20 <br /> Chromium 5.0 B 49.3 48.2 mg/Kg 88 75-125 2 20 <br /> Cobalt 1.4 49.3 45.0 mg/Kg 88 75-125 3 20 <br /> Copper 4.6 49.3 49.6 mg/Kg 91 75-125 1 20 <br /> Lead 2.4 49.3 46.5 mg/Kg 90 75-125 2 20 <br /> Molybdenum ND 49.3 38.8 mg/Kg 79 75-125 3 20 <br /> Nickel 3.8 49.3 49.2 mg/Kg 92 75-125 2 20 <br /> Selenium ND 49.3 43.6 mg/Kg 88 75-125 3 20 <br /> Silver ND 24.6 22.2 mg/Kg 90 75-125 3 20 m <br /> Thallium ND 49.3 41.6 mg/Kg 84 75-125 5 20 <br /> Vanadium 11 49.3 54.7 mg/Kg 88 75-125 1 20 <br /> Zinc 7.7 49.3 55.8 mg/Kg 98 75-125 1 20 <br /> Method: 6020 - Metals (ICP/MS) <br /> Lab Sample ID: MB 440-482554/1-B "10 Client Sample ID: Method Blank <br /> Matrix: Solid Prep Type: TCLP <br /> Analysis Batch:482964 Prep Batch: 482800 <br /> MB MB <br /> Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac <br /> Lead ND 0.10 0.020 m9/L 06/19/18 01:24 06/19/18 13:43 10 <br /> Lab Sample ID: LCS 440-482554/2-8 "10 Client Sample ID: Lab Control Sample <br /> Matrix: Solid Prep Type: TCLP <br /> Analysis Batch:482964 Prep Batch: 482800 <br /> Spike LCS LCS %Rec. <br /> Analyte Added Result Qualifier Unit D %Rec Limits <br /> Lead 2.00 1.90 mg/L 95 -80--120 <br /> Lab Sample ID: 440-212315-1 MS Client Sample ID: UPSTKMR-572 <br /> Matrix: Solid Prep Type: TCLP <br /> Analysis Batch: 482964 Prep Batch: 482800 <br /> Sample Sample Spike MS MS %Rec. <br /> Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits <br /> Lead 0.077 J 2.00 2.00 mg/L 96 75-125 <br /> Lab Sample ID: 440-212315-1 MSD Client Sample ID: UPSTKMR-572 <br /> Matrix: Solid Prep Type: TCLP <br /> Analysis Batch: 482964 Prep Batch: 482800 <br /> Sample Sample Spike MSD MSD %Rec. RPD <br /> Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits RPD Limit <br /> Lead 0.077 J 2.00 1.98 mg/L 95 75-125 1 20 <br /> Lab Sample ID: MB 440-482522/1-A "20 Client Sample ID: Method Blank <br /> Matrix: Solid Prep Type: STLC Citrate <br /> Analysis Batch: 482987 <br /> MB MB <br /> Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac <br /> Lead ND 0.10 0.040 mg/L 06/19/1814:13 20 <br /> TestAmerica Irvine <br /> Page 24 of 32 6/19/2018 <br />