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QC Sample Results <br /> Client: GHD Services Inc. TestAmerica Job ID: 720-90502-2 <br /> Project/Site: UPRR- French Camp <br /> Method: 8260B/CA LUFTMS - 8260B / CA LUFT MS <br /> Lab Sample ID: 720-90502-5 MS Client Sample ID: HYD.WASTE <br /> Matrix: Solid Prep Type: Total/NA <br /> Analysis Batch: 257776 Prep Batch: 257729 <br /> Sample Sample Spike MS MS %Rec. <br /> Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits <br /> 1,1,1,2-Tetrachloroethane ND 4960 5290 ug/Kg 107 72-129 <br /> 1,1,1-Trichloroethane ND 4960 5320 ug/Kg 107 69-132 <br /> 1,1,2,2-Tetrachloroethane ND 4960 4370 ug/Kg 88 69-133 <br /> 1,1,2-Trichloro-1,2,2-trifluoroetha ND 4960 5830 ug/Kg 118 66-128 <br /> ne <br /> 1,1,2-Trichloroethane ND 4960 5060 ug/Kg 102 70-130 <br /> 1,1-Dichloroethane ND 4960 5190 ug/Kg 105 79-125 <br /> 1,1-Dichloroethene ND 4960 5410 ug/Kg 109 70-130 <br /> 1,1-Dichloropropene ND 4960 5160 ug/Kg 104 81-134 <br /> 1,2,3-Tri ch lorobenzene ND 4960 5300 ug/Kg 107 72-159 <br /> 1,2,3-Trichloropropane ND 4960 4560 ug/Kg 92 74-135 <br /> 1,2,4-Trichlorobenzene ND 4960 5590 ug/Kg 113 71-163 <br /> 1,2,4-Trimethylbenzene ND 4960 5190 ug/Kg 105 62-155 <br /> 1,2-Dibromo-3-Chloropropane ND 4960 5380 ug/Kg 108 52-156 <br /> 1,2-Dichlorobenzene ND 4960 5010 ug/Kg 101 77-140 <br /> 1,2-Dichloroethane ND 4960 4780 ug/Kg 96 67-126 <br /> 1,2-Dichloropropane ND 4960 5140 ug/Kg 104 70-130 <br /> 1,3,5-Tri methyl benzene ND 4960 5240 ug/Kg 106 69-142 <br /> 1,3-Dichlorobenzene ND 4960 5130 ug/Kg 103 71-135 <br /> 1,3-Dichloropropane ND 4960 4950 ug/Kg 100 73-133 <br /> 1,4-Dichlorobenzene ND 4960 5160 ug/Kg 104 76-130 <br /> 2,2-Dichloropropane ND 4960 5690 ug/Kg 115 67-146 <br /> 2-Butanone(MEK) ND 24800 24400 ug/Kg 98 58-159 <br /> 2-Chlorotoluene ND 4960 5000 ug/Kg 101 66-143 <br /> 2-Hexanone ND 24800 21100 ug/Kg 85 54-124 <br /> 4-Chlorotoluene ND 4960 5090 ug/Kg 103 73-136 <br /> 4-Isopropyltoluene ND 4960 5210 ug/Kg 100 62-153 <br /> 4-Methyl-2-pentanone(MIBK) ND 24800 21800 ug/Kg 88 53-129 <br /> Acetone ND 24800 26300 ug/Kg 106 12-234 <br /> Benzene ND 4960 5180 ug/Kg 104 76-122 <br /> Bromobenzene ND 4960 5220 ug/Kg 105 77-125 <br /> Bromoform ND 4960 5060 ug/Kg 102 54-149 <br /> Bromomethane ND 4960 4720 ug/Kg 95 14-175 <br /> Carbon disulfide ND 4960 5300 ug/Kg 107 13-151 <br /> Carbon tetrachloride ND 4960 5370 ug/Kg 108 72-136 <br /> Chlorobenzene ND 4960 5090 ug/Kg 103 81-128 <br /> Chlorobromomethane ND 4960 5440 ug/Kg 110 74-134 <br /> Chlorodibromomethane ND 4960 5590 ug/Kg 113 70-130 <br /> Chloroethane ND 4960 4510 ug/Kg 91 53-124 <br /> Chloroform ND 4960 5190 ug/Kg 105 75-133 <br /> Chloromethane ND 4960 3260 ug/Kg 66 43-146 <br /> cis-1,2-Dichloroethene ND 4960 4980 ug/Kg 100 70-130 <br /> cis-1,3-Dichloropropene ND 4960 5510 ug/Kg 111 79-144 <br /> Dibromomethane ND 4960 4820 ug/Kg 97 70-139 <br /> Dichlorobromomethane ND 4960 5240 ug/Kg 106 80-131 <br /> Dichlorodifluoromethane ND 4960 5590 ug/Kg 113 30-120 <br /> Ethylbenzene ND 4960 5200 ug/Kg 105 76-137 <br /> Ethylene Dibromide ND 4960 5170 ug/Kg 104 70-138 <br /> TestAmerica Pleasanton <br /> Page 11 of 43 1/24/2019 <br />