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1534 Willow Pass Road,Pittsburg,CA 94565-1701 _ M c C a m p b e I I Analytical, Inc. Toll Free Telephone:(877)252-9262/Fax:(925)252-9269 I "When Quality Counts" http://www.mccampbell.com/E-mail:main@mccampbell.com Quality Control Report Client: Patriot Environmental Services,Inc. WorkOrder: 2411396 Date Prepared: 11/07/2024 BatchID: 305511 Date Analyzed: 11/11/2024 Extraction Method: SW5030B Instrument: GC49 Analytical Method: SW8260D Matrix: Soil Unit: mg/kg Project: 6515;Marathon Stockton Bin Sample ID: MB/LCS/LCSD-305511 QC Summary Report for SW8260D Analyte LCS LCSD SPK LCS LCSD LCS/LCSD RPD RPD Result Result Val %REC %REC Limits Limit Acetone 0.22 0.22 0.20 108 110 60-140 1.55 30 tert-Amyl methyl ether(TAME) 0.015 0.017 0.020 74 83 50-140 11.4 30 Benzene 0.016 0.017 0.020 80 83 60-140 3.98 30 Bromobenzene 0.019 0.018 0.020 96 92 60-140 4.08 30 Bromochloromethane 0.017 0.017 0.020 84 86 60-140 2.42 30 Bromodichloromethane 0.018 0.018 0.020 91 92 60-140 0.966 30 Bromoform 0.015 0.015 0.020 76 76 40-140 0.304 30 Bromomethane 0.017 0.017 0.020 85 87 30-140 2.46 30 2-Butanone(MEK) 0.057 0.055 0.080 71 69 50-140 3.91 30 t-Butyl alcohol(TBA) 0.076 0.075 0.080 95 94 50-140 0.765 30 n-Butyl benzene 0.023 0.023 0.020 116 113 60-150 2.98 30 sec-Butyl benzene 0.023 0.023 0.020 116 113 60-150 2.41 30 tert-Butyl benzene 0.022 0.022 0.020 109 108 60-140 0.777 30 Carbon Disulfide 0.017 0.017 0.020 83 87 50-140 4.90 30 Carbon Tetrachloride 0.018 0.019 0.020 88 94 60-140 6.94 30 Chlorobenzene 0.018 0.018 0.020 90 90 60-140 0.417 30 Chloroethane 0.016 0.016 0.020 78 80 50-140 2.89 30 Chloroform 0.017 0.018 0.020 87 90 60-140 2.94 30 Chloromethane 0.018 0.019 0.020 92 97 20-140 5.26 30 2-Chlorotoluene 0.021 0.021 0.020 107 106 60-140 0.908 30 4-Chlorotoluene 0.022 0.021 0.020 109 106 60-140 3.13 30 Dibromochloromethane 0.017 0.017 0.020 87 87 50-140 0.344 30 1,2-Dibromo-3-chloropropane 0.0092 0.0085 0.010 92 85 30-140 7.77 30 1,2-Dibromoethane(EDB) 0.010 0.0098 0.010 101 98 40-140 3.10 30 Dibromomethane 0.017 0.018 0.020 85 88 60-140 3.00 30 1,2-Dichlorobenzene 0.016 0.016 0.020 82 80 60-140 2.24 30 1,3-Dichlorobenzene 0.019 0.019 0.020 97 96 60-140 1.08 30 1,4-Dichlorobenzene 0.019 0.019 0.020 95 93 60-140 2.19 30 Dichlorodifluoromethane 0.0056 0.0057 0.020 28 28 10-140 1.46 30 1,1-Dichloroethane 0.017 0.018 0.020 85 88 60-140 3.98 30 1,2-Dichloroethane(1,2-DCA) 0.017 0.018 0.020 87 90 60-140 2.85 30 1,1-Dichloroethene 0.017 0.018 0.020 85 89 60-140 4.27 30 cis-1,2-Dichloroethene 0.017 0.018 0.020 87 91 60-140 3.83 30 trans-1,2-Dichloroethene 0.017 0.018 0.020 87 89 60-140 3.34 30 1,2-Dichloropropane 0.017 0.017 0.020 84 86 60-140 2.44 30 1,3-Dichloropropane 0.018 0.018 0.020 88 89 60-140 0.123 30 2,2-Dichloropropane 0.019 0.020 0.020 95 100 60-140 5.19 30 1,1-Dichloropropene 0.018 0.018 0.020 88 92 60-140 4.74 30 (Cont.) CA ELAP 1644•NELAP 4033ORELAP Page 15 of 27