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CLIENT: WET Laboratory ANALYTICAL QC SUMMARY REPORT <br /> Work Order: N081747 <br /> Project: KIRK, 26020676S TestCode: 8270E_S <br /> Sample ID: MB-128843 SampType:MBLK TestCode:8270E_S Units: Ng/Kg Prep Date: 3/2/2026 RunNo: 216165 <br /> Client ID: PBS Batch ID: 128843 TestNo:EPA 8270E EPA 3546 Analysis Date: 3/2/2026 SegNo: 7498689 <br /> Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual <br /> Surr: 2-Fluorophenol 3079.500 5000 61.6 21 120 <br /> Surr: 4-Terphenyl-d14 6021.500 5000 120 28 128 <br /> Surr: Nitrobenzene-d5 4219.500 5000 84.4 22 120 <br /> Surr: Phenol-d5 3312.000 5000 66.2 22 120 <br /> Sample ID: N081751-005A-MS SampType:MS TestCode:8270E_S Units: Ng/Kg Prep Date: 3/2/2026 RunNo: 216165 <br /> Client ID: ZZZZZZ Batch ID: 128843 TestNo:EPA 8270E EPA 3546 Analysis Date: 3/2/2026 SegNo: 7498695 <br /> Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual <br /> 1,2,4-T rich lorobenzene 4948.474 330 5003 0 98.9 37 120 <br /> 1,2-Dichlorobenzene 3952.976 330 5003 0 79.0 36 120 <br /> 1,3-Dichlorobenzene 3706.353 330 5003 0 74.1 35 120 <br /> 1,4-Dichlorobenzene 3825.913 330 5003 0 76.5 35 120 <br /> 2,4,5-T rich lorophenol 5160.580 330 5003 0 103 22 120 <br /> 2,4,6-T rich lorophenol 5375.188 330 5003 0 107 18 120 <br /> 2,4-Dichlorophenol 4931.966 1700 5003 0 98.6 23 120 <br /> 2,4-Diin ethyl phenol 4269.135 330 5003 0 85.3 26 120 <br /> 2,4-Dinitrophenol 1951.976 1700 5003 0 39.0 0 120 <br /> 2,4-Dinitrotoluene 5082.041 330 5003 0 102 36 120 <br /> 2,6-Dinitrotoluene 4865.433 330 5003 0 97.3 36 120 <br /> 2-Chloronaphthalene 4881.941 330 5003 0 97.6 40 120 <br /> 2-Chlorophenol 3982.991 330 5003 0 79.6 29 120 <br /> 2-Methyl naphthalene 4659.330 330 5003 0 93.1 39 120 <br /> 2-Methylphenol 3853.927 330 5003 0 77.0 33 120 <br /> 2-Nitroaniline 5144.072 1700 5003 0 103 30 120 <br /> 2-Nitrophenol 4387.694 330 5003 0 87.7 24 120 <br /> 3,3"-Dichlorobenzidine 6415.708 660 7504 0 85.5 11 128 <br /> 3-Nitroaniline 4291.146 1700 5003 0 85.8 39 120 <br /> 4,6-Dinitro-2-methyl phenol 3859.930 1700 5003 0 77.2 14 120 <br /> 4-Bromophenyl-phenylether 5382.191 330 5003 0 108 36 120 <br /> Qualifiers: <br /> B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded <br /> ND Not Detected at the Reporting Limit R RPD outside accepted recovery limits S Spike/Surrogate outside of limits due to matrix interference <br /> DO Surrogate Diluted Out Calculations are based on raw values (M) Test is modified <br /> CALIFORNIA I P:562.219.7435 F:562.219.7436 NEVADA I P:702.307.2659 F:702.307.2691 <br /> ASSET I,A BORATORI E5 11110 Artesia Blvd.,Ste B,Cerritos,CA 90703 3151 W.Post Rd.,Las Vegas,NV 89118 <br /> ELAP Cert 2921 ELAP Cert 2676 I NV Cert NVO0922 <br /> "Serving Clients with Passion and Professionalism" NV Cert CA01638 ORELAP Cert 4046 <br /> 12 of 17 <br />