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CLIENT: WET Laboratory ANALYTICAL QC SUMMARY REPORT <br /> Work Order: N081747 <br /> Project: KIRK, 26020676S TestCode: 8270E_S <br /> Sample ID: N081751-005A-MS SampType:MS TestCode:8270E_S Units: Ng/Kg Prep Date: 3/2/2026 RunNo: 216165 <br /> Client ID: ZZZZZZ Batch ID: 128843 TestNo:EPA 8270E EPA 3546 Analysis Date: 3/2/2026 SegNo: 7498695 <br /> Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual <br /> Hexachlorobenzene 5593.797 330 5003 0 112 38 120 <br /> Hexachlorobutadiene 5590.795 660 5003 0 112 38 120 <br /> Hexachlorocyclopentadiene 5217.109 660 5003 0 104 23 120 <br /> Hexachloroethane 3967.984 330 5003 0 79.3 34 120 <br /> Indeno(1,2,3-cd)pyrene 4660.330 330 5003 0 93.2 27 120 <br /> Isophorone 4932.466 330 5003 0 98.6 17 144 <br /> N-Nitrosodi-n-propylamine 4588.294 330 5003 0 91.7 36 120 <br /> N-Nitrosodiphenylamine 4648.324 330 5003 0 92.9 39 120 <br /> Naphthalene 4277.639 330 5003 0 85.5 36 120 <br /> Nitrobenzene 4607.804 330 5003 0 92.1 37 120 <br /> Pentachlorophenol 4462.231 1700 5003 0 89.2 8 120 <br /> Phenanthrene 4683.842 330 5003 0 93.6 23 127 <br /> Phenol 3820.910 330 5003 0 76.4 30 120 <br /> Pyrene 4447.224 330 5003 0 88.9 18 122 <br /> Pyridine 2995.998 1700 7504 0 39.9 7 120 <br /> Surr: 1,2-Dichlorobenzene-d4 3274.637 5003 65.5 26 120 <br /> Surr: 2,4,6-Tribromophenol 3952.976 5003 79.0 31 120 <br /> Surr: 2-Chlorophenol-d4 2801.401 5003 56.0 24 120 <br /> Surr: 2-Fluorobiphenyl 4051.526 5003 81.0 28 120 <br /> Surr: 2-Fluorophenol 2557.779 5003 51.1 21 120 <br /> Surr: 4-Terphenyl-d14 3474.737 5003 69.5 28 128 <br /> Surr: Nitrobenzene-d5 3741.371 5003 74.8 22 120 <br /> Surr: Phenol-d5 2646.323 5003 52.9 22 120 <br /> Sample ID: N081751-005A-MSD SampType:MSD TestCode:8270E_S Units: Ng/Kg Prep Date: 3/2/2026 RunNo: 216165 <br /> Client ID: ZZZZZZ Batch ID: 128843 TestNo:EPA 8270E EPA 3546 Analysis Date: 3/2/2026 SegNo: 7498696 <br /> Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual <br /> 1,2,4-T rich lorobenzene 5052.052 330 5005 0 101 37 120 4948 2.07 20 <br /> 1,2-Dichlorobenzene 3963.964 330 5005 0 79.2 36 120 3953 0.278 20 <br /> Qualifiers: <br /> B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded <br /> ND Not Detected at the Reporting Limit R RPD outside accepted recovery limits S Spike/Surrogate outside of limits due to matrix interference <br /> DO Surrogate Diluted Out Calculations are based on raw values (M) Test is modified <br /> CALIFORNIA I P:562.219.7435 F:562.219.7436 NEVADA I P:702.307.2659 F:702.307.2691 <br /> ASSET I,A 6ORATORI E5 11110 Artesia Blvd.,Ste B,Cerritos,CA 90703 3151 W.Post Rd.,Las Vegas,NV 89118 <br /> ELAP Cert 2921 ELAP Cert 2676 I NV Cert NVO0922 <br /> "Serving Clients with Passion and Professionalism" NV Cert CA01638 ORELAP Cert 4046 <br /> 14 of 17 <br />