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Table 2.4:Sample Containers,Preservation,Holding Times,and Analytical Methods <br /> DetailsSampling and Container <br /> Asbestos -.-e Soil Lead B...d sttamt Water Soil:High Level Sol]:Loss,Level Lead Based Paint Wot,r Soil Lead Based Point <br /> and Asbe and Asbestos and Asbestos <br /> (3)40-m glass VOA vials Add 5 g soil f 40, Add 5g soil to 40-ad. 14 days if chilled f 5 6-C, <br /> (3)40.mL glass VOA vial, soul Na to 48 HCIpH<2, alpre-pres erved ftozwwif <br /> (wif ath bar fr low-level VOA vial pre-preserved VOAvi 7 a(wgrreaerved); and fen Na VOC SW8260B SW8260B Na Na PTFE septum caps;ro av der <6°C, wifad.water hours; <br /> bubbles soil),PTFE septum caps: m headspace wrath 10 mL mefaml, sodi 5 mumbisulfate, 144 days(preserved) 14 days ifpreaerved toT—Cwe®sampler 5 6 c 6-C mef—1 or wif bisulfate in <br /> (1)4 oa glassjar wif 7 days to extraction; 14 days to ext fi-o; <br /> SVOC SW8270C SW82]OC der der (2)1-L amber glass bottle Teflo dD lined lid der <_6°C <_6°C <_6°C der 40 days to analysis 40 days to analysis der <br /> (3)40.mL glass VOA vials Add 5 g soil to 40, Add 59 wil to 40-mL 14 days if chilled to<6°C, <br /> (2)40-mL glass VOA vial, HCI pH<2, VOA vial pro-preserved and fen fozen within 48 <br /> (with stn bar for low-level VOA vial pre-preserved with 5 mL water and Na 14 der TPH-GRO SW8015M SW8015M der der PTFE septum caps;roav der <_6°C, days hours; der <br /> bubbles soil),PTFE septum caps: m headspace wrath 10 6 methaml, sodium bisulf te, 14 days ifpreserved in <br /> TemaCore®sampler <6°C <6°C methanol or with bisulfate to <br /> glass (1)4 oa glassjar with 7 days to extraction; 14 days to extraction; <br /> TPH-DRO/RRO SW8015M SW8015M Na Na (1)1-L amber bottle Teflon lined lid Na <6°C <6°C <6°C Na 40 der to ana is 40 der s to anal sis Na <br /> (1)4 oz glassjar wif, 7 days to exhrction; 14 days to exkactioq <br /> PeaRcidea SW8081H SW8081H der der (1)1-L amber glass bottle der <_6°C <_6°C <_6°C der der <br /> Teflors8lined lid 40 der f—is 40 der to arel is <br /> (1)4 oa glassjar with 7 days to extraction; 14 days to extracting <br /> Herbicides 3W8151A 9W8I5IA Na Na (1)1-L amber glass bottle Na <6°C <6°C <6°C Na jWaTeflarvB lined lid 40 der [o ana is 40 der s to anal sis(1)4ozglassjarwif 7days to exhrctog 14 days to extrctoq <br /> PCBs SW8082A SW8082A der der (1)1-L aber glass bottle da <_6°C <_6-C <_6°C derTeflors8lined lid 40 der f ana 40der to arel isTotal Metal,(CAM 17) SW6010C/6020A SW6010C/6020A/7471A da der (1)500-mL HDPE book (1)4oa glassjar with da HNO,t to pH<2 <6 <6°C der I80 days ftom sample 180 days ftom sample/7470A Teflon lined lid nott — not ftozen eoflection untilanalysisc U_ionumilanalysis <br /> SW6010C/6020A (1)500.mL HDPE bottle HNO,topH<2 180 days ftom sample <br /> Diolved Meta6 7470A der der der Field filter der da Field filter Na der der eoflectionwrtil analysis Na <br /> 8015M(GRO/DRO/RRO); <br /> Investigation Dcrivctl Waste (5)4 oz glassjar wif Holding time per the standard <br /> Charae[crivstioo Na 6010/6020(RC mend RA 8 s); Na Na Na Na Wa <6°C <6°C Wa Wa Wa <br /> 9095A(paint filter-flee liquid); TeflorsID lined lid method mquirement <br /> Ninote/Nitrite as Nitrogen E300.0 E300.0 Na Na (1)500—L HDPE bottle (1 T4fl gl lined tldth Na <6°C Na Wa Wa 48 bows to analysis 7 days Wa <br /> (1)500 mL HDPE jar with 28 days at56-C,or 90 <br /> PFAS der Draft Mefod 1633 da der (2)500.mL HDPE bottle Ilnerlesa HDPE or der <6°C <6-C <6-C der 90 days Na <br /> polypropykm cap days frozen at-20-C <br /> Total D'asnlved Solids(TDS) E160.1 Wa Na Na (1)500-mL HDPE bottle Field filter Na Na <6°C Na Na Na 7 days toanalysis Na Na <br /> Hardne„ SM2340B der Iva der (1)250.mL HDPE bottle der der "NO, <br /> ro pH<2, Na der der I80 days ftom sample Na Na <br /> <6°C eoflection until analysis <br /> Binchemi-I Oxygen Demand(BOD) SM5210B Wa Na de (1)1-L HDPE bottle Wa Na <6°C Na Wa Wa 48 bows to analysis Na Wa <br /> pH SM4500H+B SW9040/9045 der der (1)250-nE HDPE both TeFlo ID. (1)4 ov lined lid jar with da <_6°C <_6-C <_6-C der hnmedianly der der <br /> � <br /> Lead Based Paint Na Wa SW 849 3050B/7000B Na Na tr/a Plastic Bag Wa Na Wa Na Wa Na Wa <br /> Asbestos Na Wa Na 600/R-93-116 Na Wa Plastic Bag Wa Na Wa Wa Wa Na Wa <br /> Acronyms and Abbreviations: <br /> <=leas than Wa=not applicable <br /> <_=kssthanorequd to Poly=polypropylero <br /> °C=degree Celsius pH=potential hydrogen <br /> DRO=diesel range organics PTFE=Teflodo- <br /> g=gram RCRA=Resoace Conservation and Recovery Act <br /> GRO-gasolirs,range organics RFI=RCRA Facility lmestigahan <br /> HDPE=high density polyefylem SVOC=semi-volatile organic coW." <br /> H2SG4=sulfuric acid TCLP=toxicity characteristicleachinglooted— <br /> HCI=hydrochloric acid Temp=t—Pt—e <br /> HNO3=nitric acid VOA=volatile organic analyze <br /> L=liter VOC=volatile organic compouM <br /> mL=milliliter <br /> nano=miwmetw <br />