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' a <br /> APEX ENVIROTECN INC. Upon removal from the steel rods,approximately the bottom <br /> s six inches of each tube Is out off and capped to be potentially <br /> STANDARD OPERATING PROCEDURES submitted for analysis. The tubes capped with aluminum <br /> foil or`Teflon"sheets and plastic caps or the samples are <br /> SOP-1 extruded from the tubes and sealed within other appropriate, <br /> HOLLOW STEM AUGER SOIL BORING SAMPLING cleaned sample containers. The samples are then <br /> hermetically sealed,labeled,and refrigerated for delivery, <br /> During drilling,soil samples for chemical analysis are under strict chain-of-custody,to the analytical laboratory. <br /> collected In thin-walled brass tubes,of varying diameters These procedures minimize the potential for cross- <br /> and lengths(e.g.,four or six inches long by two inches contamination and volatilization of volatile organic <br /> outside diameter). Three or four of the selected tubes,plus compounds(VOC)prior to chemical analysis. <br /> a spacer tube,are set in an 18-inch long split-barrel sampler <br /> of the appropriate inside-diameter. The remaining portion of the plastic tube is cut open and a <br /> portion of the soil sample collected at each sampling interval <br /> Where possible,the spit-barrel sampler is driven its entire is analyzed in the field using either a portable PiD,FID, <br /> length either hydraulically or using a 140-pound drop organic vapor analyzer,catalytic gas detector,or an <br /> hammer. The sampler Is extracted from the borehole and explosimeter. The purpose of this field analysis is to <br /> the brass tubes,containing the sail samples,are removed. qualitatively determine the presence or absence of <br /> Upon removal from the sampler,the selected brass tubes hydrocarbons,and the samples to be analyzed at the <br /> are either immediately trimmed and capped with aluminum laboratory. The soil sample is sealed in either a glass jar or <br /> foil or'Teflon*sheets and plastic caps or the samples are plastic bag to allow for some volatilization of VOC. The PID <br /> extruded from the tubes and sealed within other appropriate, is then used to measure the concentrations of hydrocarbons <br /> cleaned sample containers. The samples are then within the container's headspace. The data is recorded on <br /> hermetically sealed,labeled,and refrigerated for delivery, both field notes and the boring logs at the depth <br /> under strict chain-of-custody,to the analytical laboratory. corresponding to the sampling point. <br /> These procedures minimize the potential for cross- <br /> contamination and volatilization of volatile organic Other soil samples are collected to document the soil and/or <br /> compounds(VOC)prior to chemical analysis. stratigraphic profile beneath the project site,and estimate <br /> the relative permeability of the subsurface materials. All <br /> One soil sample collected at each sampling Interval is drilling and sampling equipment are either steam cleaned or <br /> analyzed In the field using either a portable photo Ionization washed in solution and doubly rinsed in delonized water <br /> detector(PiD),flame ionization detector(FID),organic vapor prior to use at each site and between boreholes to minimize <br /> analyzer,catalytic gas detector,or an explosimeter. The the potential for cross-contamination. <br /> purpose of this field analysis is to qualitatively determine the <br /> presence or absence of hydrocarbons,and the samples to In the event the soil samples cannot be submitted to the <br /> be analyzed at the laboratory. The soil sample is sealed in analytical laboratory on the same day they are collected <br /> either a brass tube,glass jar,or plastic bag to allow for some (e.g.,due to weekends or holidays),the samples are <br /> volatilization of VOC. The PID is then used to measure the temporarily stored until the first opportunity for submittal <br /> concentrations of hydrocarbons within the container's either on ice in a cooler,such as when in the field,or in a <br /> headspace. The data is recorded on both field notes and the refrigerator at Apex's office. <br /> boring fogs at the depth corresponding to the sampling point. <br /> SOP•3 <br /> Other soil samples are collected to document the soil and/or SOIL EXCAVATION AND SAMPLING <br /> stratigraphic profile beneath the project site,and estimate <br /> the relative permeability of the subsurface materials. All Excavation and subsequent soil sampling Is performed <br /> drilling and sampling equipment are either steam cleaned or under the direction of a registered geologist or civil engineer. <br /> washed in solution and doubly rinsed in defonized water To reduce the potential for cross-contamination,all <br /> prior to use at each site and between boreholes to minimize excavation equipment is either steam cleaned or washed <br /> the potential for cross-contamination. prior to use and between excavations. Soil samples for <br /> chemical analysis are collected in cleaned,thin-walled brass <br /> In the event the soil samples cannot be submitted to the tubes of varying diameters and lengths(e.g.,six inches long <br /> analytical laboratory on the same day they are collected by two inches outside diameter)or other appropriate cleaned <br /> (e.g.,due to weekends or holidays),the samples are sample container. If used,one tube may be set in a two inch <br /> temporarily stored until the first opportunity for submittal Inside diameter,hand-driven sampler. To reduce the <br /> either on ice In a cooler,such as when In the field,or in a potential for cross-contamination between samples,the <br /> refrigerator at Apex's office. sampler is washed in a solution and doubly rinsed between <br /> each sampling event. <br /> SOP-2 <br /> DIRECT PUSH SOIL BORING SAMPLING Upon recovery,a portion of the soil sample is sealed for later <br /> screening with either a portable PID,FID,or an <br /> During drilling,soil samples for chemical analysis are explosimeter. Another portion of the sample is used for <br /> collected in thin-walled plastic tubes,of varying diameters description of the excavated materials. A third portion of the <br /> and lengths(e.g.,two inches outer diameter by four feet sample Is hermetically sealed,labeled and refrigerated for <br /> long). The plastic sampling tube is placed inside a steel rod delivery,under strict chain-of-custody,to the analytical <br /> and driven into the subsurface to the desired depth using a laboratory. These procedures minimize the potential for <br /> direct push drill rig. The steel rod is then removed from the cross-contaminatlon and volatilization of volatile organic <br /> subsurface and the plastic tube containing the soil sample compounds prior to chemical analysis. <br /> are removed from the steel rod. The process is repeated <br /> until the desired depth of the boring is reached. In the event the soil samples cannot be submitted to the <br /> analytical laboratory on the same day they are collected <br /> (e.g..due to weekends or holidays),the samples are <br />