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Alpha Analytical, Inc 255 Glendale Ave • Suite 21 • Sparks,Nevada 89431-5778 L (775)355-1044 • (775)355-0406 FAX • 1-800-283-1183 Uate T11111a Re Work Order 10-Se -OZ QC Summary p 02090341 Method Blank Type MBLK Test Code SW8015 Batch ID MSIW0904B File ID C 1HPCHEM1MS011DATA1020904102090407 D Analysis Date 09/04/2002 14 23 Sample ID MBLK MSlW0904B Units pg/L Run ID GCIMSD_1_020904A Prep Date 09/04/2002 Analyte Result PQL SpkVal SpkRefVal %REC LowLimit HighLimit RPD Ref Val %RPD Qual TPH Purgeable ND 50 Surr 1 2-Dichloroethane-d4 9 82 10 98 71 130 Surr Toluene-d8 104 10 104 69 127 Surr 4-Bromofluorobenzene 9 3 10 93 80 123 Laboratory Control Spike Type LCS Test Code SW8015 Batch ID MSIW0904B File ID C 1HPCHEM1MS011DATA1020904102090405 D Analysis Date 09104/200213 31 Sample ID GLCSMSIW0904B Units pglL Run ID GCIMSD_1_020904A Prep Date 09104/2002 Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighLimit RPD Ref Val %RPD Qual TPM Purgeable 436 50 400 109 58 136 Surr 1 2-Dichloroethane-d4 966 10 97 71 130 Surr Toluene-dB 106 10 106 69 127 Surr 4-Bromofluorobenzene 951 10 95 80 123 Sample Matrix Spike Type MS Test Code SW8015 Batch ID MSlW0904B File ID C kHPCHEMkMS01%DATAk020904W2D90428 D Analysis Date 09/04/2002 23 23 Sample ID 02090306-01AGS Units pg1L Run ID GC/MSD_1_020904A Prep Date 09/04/2002 Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighLimit RPD Ref Val %RPD Qual TPH Purgeable 406 50 400 0 102 58 136 Surr 1,2-Dichloroethane-d4 109 10 109 71 130 Surr Toluene-d8 989 10 99 69 127 urr 4-Bromofluorobenzene 926 10 93 80 123 ample Matrix Spike Duplicate Type MSD Test Code SW8015 Batch ID MSIWD904B File ID C IHPCHEMkMS01kDATAk020904k02090429 D Analysis Date 09104/2002 23 49 Sample ID 02090306-01AGSD Units pg/L Run ID GG/MSD_1_020904A Prep Date 09/0412002 Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit Highl-=t RPD Ref Val %RPD Qual TPH Purgeable 410 50 400 0 103 58 136 406 1 1 Surr 1 2-Dichloroethane-d4 107 10 107 71 130 Surr Toluene-dB 103 10 103 69 127 Surr 4-Bromofluorobenzene 953 10 95 80 123 Comments ND-Not Detected at the Reporting Limit D-If the spiked value is<25%of the reference value,recovery should not be calculated S-Spike Recovery outside accepted recovery limits M-Spike Recovery outside accepted recovery limits due to matrix 13-Analyte detected in the associated Method Blank Reported in micrograms per liter,per client request