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COLUMBIA ANALYTICAL SERVICES,INC <br /> QA/QC Deport <br /> Client CMCON Service Request S9900683 <br /> Protect Apac.lie PI&AILJ22640-100 001 Date Collected NA <br /> Sample Matrix SOd Date Received NA <br /> Date Extracted NA <br /> Date Analyzed NA <br /> Surrogate Recovery Summary <br /> Fuel Oxygenates <br /> Prep Method NONE Units PERCENT <br /> Andlysis Method 8260 Basis NA <br /> Test P e r c e n t R e c o v e r y <br /> Sample Name Lai) Code Notes Dibramofluoromethane Toluene-D8 4-Bromofluorobenzene <br /> B-1(82) 59900683-008 98 106 107 <br /> B-2(102) 59900683-012 99 105 105 <br /> Method Blank(MSD 1) S9903 l0-WB 1 99 104 105 <br /> Method Blank(STLC BLK) 5990306-WB 1 99 104 105 <br /> is <br /> RPA ALLeptance Limits 86-118 88-110 86-115 <br /> 0 SUFl11020597p <br /> Page 52 <br />