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COLUMBIA ANALYTICAL SERVICES, INC <br /> Analytical Report <br /> Client EMCON Service Request 59900683 <br /> Project Apache Plastic,,/22640-100 001 Date Collected NA <br /> Sample Mate ea Soil Date Received NA <br /> Fuel Oxygenates <br /> Sample Name Method Blank Units ug/Kg(ppb) <br /> Lab Code 5990304-SB I Basis Wet <br /> Test Notes <br /> Pe ep Analysis Dilution Date Date Result <br /> Analyte Method Method MRL Factor Extracted Analyzed Result Notes <br /> tert-Butyl Alcohol NONE 8260 500 1 3/4199 3/4199 ND <br /> Methyl tert-Butyl Ethe, NONE 8260 5 1 3/4/99 3/4/99 ND <br /> Ditsopropyl Ether NONE 8260 50 1 3/4/99 3/4/99 ND <br /> Ethyl tert-Butyl Ether NONE 8260 50 1 3/4/99 3/4/99 ND <br /> tert-Amyl Methyl Ether NONE 8260 50 1 3/4/99 3/4/99 ND <br /> Ethanol NONE 8260 5000 1 3/4/99 3/4/99 ND <br /> 1544/021A97p <br /> Page 12 <br />