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COLUMBIA ANALYTICAL SERVICES,INC <br /> Analytical Report <br /> Client EMCON Service Request 59900683 <br /> Project Apache Plastics/22640-100 001 Date Collected 2/23/99 <br /> Sample Matt ix Water Date Received 3/2/99 <br /> Fuel Oxygenates <br /> Sample Name E Ili-l(l 00) Units ug/L(ppb) <br /> Lab Code 59900683-015 Basis NA <br /> Test Notes Ml <br /> Pri p Analysts Dilution Date Date Result <br /> Analyte Method Method MRL Factor Extracted Analyzed Result Notes <br /> Cert-Butyl Alcohol NONE 8260 50 10 NA 3/5/99 <500 <br /> Methyl tert-Butyl Ether NONE 8260 0 5 10 NA 3/5/99 <5 <br /> Dusopropyl Ether NONE 8260 5 10 NA 3/5/99 <50 <br /> Ethyl tert-Butyl Ether NONE 8260 5 10 NA 3/5/99 <50 <br /> tert-Amyl Methyl Ethel NONE 8260 5 10 NA 3/5/99 <50 <br /> Ethanol NONE 8260 500 10 NA 3/5/99 <5000 <br /> M1 The MRL was elevated because of matrix interferences <br /> The sample conlomed high concentrations of petroleum hydrocarbons <br /> 11,44/021197p <br /> Page 14 <br />