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COLUMBIA ANALYTICAL SERVICES,INC <br /> Analytical Deport <br /> Client EMCON Service Request S9900683 <br /> P1;olect Apache.Plastic,,/22640-1 00 001 Date Collected NA <br /> Sample Matl la Writer Date Received NA <br /> Fuel Oxygenates <br /> Sample Name Method Blank(MSDI) Units ug/L(ppb) <br /> Lab Code S990304-WB1 Basis NA <br /> Test Notes <br /> Pi ep Analysis Dilution Date Date Result <br /> Analyte M(,thod Method MRL Factor Extracted Analyzed Result Notes <br /> tert-Butyl Alcohol NONE 8260 50 1 NA 3/4/99 ND j <br /> Methyl Cert-Butyl RIM NONE 8260 05 1 NA 3/4/99 ND <br /> Di sopropyl Ether NONE 8260 5 1 NA 3/4/99 ND <br /> Ethyl Cert-Butyl Ether NONE 8260 5 1 NA 3/4/99 ND <br /> Cert-Amyl Methyl Ether NONE 8260 5 1 NA 3/4/99 ND <br /> Ethanol NONE 8260 500 1 NA 3/4/99 ND <br /> 1M4/021197p <br /> Page 19 <br />