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COLUMBIA ANALYTICAL SERVICES,INC <br /> Analytical Report <br /> . Client EMOON Service Request S9900683 <br /> Protect Apache Plastics/22640-100 001 Date Collected 2/22/99 <br /> Sample Matrix Sod Date Received 3/2/99 <br /> BTEX,MTBE and TPH as Gasoline <br /> Sample Name B-2(102) Units mg/Kg(ppm) <br /> Lab Code 59900683-012 Basis Wet <br /> Test Notes <br /> Prep Analysts Dilution Date Date Result <br /> Analyte Method Method MRI, Factor Extracted Analyzed Result Notes <br /> TPH as Gasoline EPA 5030 CA/LUFT 1 1 3/4/99 3/6199 ND <br /> Benzene EPA 5030 8020 0 005 1 3/4/99 3/6/99 0 049 <br /> Toluene EPA 5030 8020 0 005 1 3/4/99 3/6/99 0 025 <br /> Ethylbenzene EPA 5030 8020 0 005 1 3/4/99 3/6/99 0 016 <br /> Xylenes,Total EPA 5030 8020 0 005 1 314/99 3/6/99 0 019 <br /> Methyl tent-Butyl Ether EPA 5030 8020 005 1 3/4/99 3/6/99 ND <br /> • <br /> • 1$227020547p <br /> Page 32 <br />