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COLUMBIA ANALYTICAL SERVICES, INC <br /> Analytical lam'eport <br /> • Client I.MCUN Service Request 59900683 <br /> Protect Apache.P1astics/22640-100 001 <br /> Date Collected NA <br /> Sample Matrix Srnl Date Received NA <br /> BTEX,MTBE and TPH as Gasoline <br /> Sample Name Method Blank Units mg/Kg(ppm) <br /> Lab Code 5990306-b61 Basis Wet <br /> Test Notes <br /> Prep Analysts Dilution Date Date Result <br /> Analyte Method Method MRL Factor Extracted Analyzed Result Notes <br /> TPH as Gasoline CPA 5030 CAlLUFT l l 3/4/99 3/8/99 ND <br /> Benzene EPA 3030 8020 0 005 l 3/4/99 3/8/99 ND <br /> Toluene EPA 5030 8020 0 005 1 3/4/99 3/8/99 ND <br /> Ethylbenzene CPA 5030 8020 0 005 1 3/4/99 3/8/99 ND <br /> Xylenes,Total EPA 3030 8020 0 005 1 3/4/99 3/8/99 ND <br /> Methyl tent-Butyl Eflier EPA 5030 8020 005 1 3/4/99 3/8/99 ND <br /> • <br /> 1522/020597p <br /> Page 35 <br />