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LancasterAnalysis Report <br />f Laboratories Y p <br />2425 New Holland Pike, PO Box 12425, Lancaster, PA 17605-2425 •717-656-2300 Fax: 717-656-2661- www,lancasterlabs.com <br />Page 3 of 3 <br />Quality <br />Control Summary <br />f <br />Client Name: ChevronTexaco <br />Group Number: 856727 <br />Reported: 06/30/03 at 12:23 AM <br />Surrogate <br />Quality Control <br />Limits: 72-128 <br />Analysis Name: BTEX + oxygenates by 8260B <br />Batch number: P031781AA <br />Dibromofluoromethane <br />1,2--Dichloroethane-d4 <br />Toluene -de <br />4-Bromofluorobenzene <br />4069283 97 <br />99 <br />99 <br />99 <br />92 <br />94 <br />Blank 98 <br />96 <br />99 <br />104 <br />98 <br />LCS 97 <br />MS 96 <br />99 <br />103 <br />95 <br />MSD 97 <br />98 <br />102 <br />97 <br />Limits: 81-120 <br />82-112 <br />85-112 <br />83-113 <br />Analysis Name: BTEX + oxygenates by 8260B <br />Batch number: P031782AA <br />Dibromofluoromethane <br />1,2-Dichloroethane-d4 <br />Toluene -d8 <br />4-Bromofluorobenzene <br />4069264 102 <br />103 <br />101 <br />101 <br />93 <br />93 <br />4069285 103 <br />107 <br />108 <br />loo <br />92 <br />4069266 105 <br />101 <br />100 <br />93 <br />4069287 103 <br />106 <br />102 <br />94 <br />Blank 105 <br />102 <br />96 <br />94 <br />LCS 103 <br />MS 103 <br />102 <br />99 <br />99 <br />JMSD 100 <br />105 <br />99 <br />99 <br />I <br />Limits: 61-120 <br />82-112 <br />85-112 <br />83-113 <br />*- Outside of specification <br />(1) The result for one or both determinations was less than five times the LOQ. <br />(2) The background result was more than four times the spike added. <br />