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Lancaster Laboratories <br />Where qualltyis a science. <br />Quality Control Summary <br />Client Name: ChevronTexaco Group Number: 826433 <br />Reported: 10/21/02 at 02:55 AM <br />Surrogate Quality Control <br />Analysis Name: BTEX + Oxygenates by 8260B <br />Batch number: N022851AB <br />Page 3 of 3 <br />r� <br />*- Outside of specification <br />)(1) The result for one or both determinations was less than five times the LOQ. <br />The background result was more than four times the spike added. <br />Lancaster Laboratories, Inc. <br />M E M B I- R 2423 New Holland Pike <br />PO Box 12425 <br />Lancaster, PA 17605-2425 <br />717-656-2300 Fax. 717-656-Z681 2216 Rev. 9111/00 <br />Dibromofluoromethane <br />1,2-Dichloroethane-d4 <br />Toluene -d8 <br />4-Bromofluorobenzene <br />3916994 <br />3916995 <br />3916996 <br />3916997 <br />3916998 <br />Blank <br />LC S <br />MS <br />MSP <br />99 <br />100 <br />99 <br />99 <br />99 <br />99 <br />97 <br />96 <br />96 <br />94 <br />93 <br />95 <br />94 <br />93 <br />94 <br />95 <br />94 <br />94 <br />99 <br />100 <br />100 <br />99 <br />99 <br />99 <br />103 <br />101 <br />101 <br />95 <br />95 <br />95 <br />94 <br />94 <br />94 <br />1,04 <br />104 <br />104 <br />Limits: <br />86-118 <br />80-120 <br />88-110 <br />86-115 <br />r� <br />*- Outside of specification <br />)(1) The result for one or both determinations was less than five times the LOQ. <br />The background result was more than four times the spike added. <br />Lancaster Laboratories, Inc. <br />M E M B I- R 2423 New Holland Pike <br />PO Box 12425 <br />Lancaster, PA 17605-2425 <br />717-656-2300 Fax. 717-656-Z681 2216 Rev. 9111/00 <br />