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IfLancaster Laboratories <br />Where quality is a science. <br />Lancaster Laboratories Sample No. WW 3926510 <br />Collected:10/22/2002 11:30 by ST <br />Submitted: 10/24/2002 09:10 <br />Reported: 11/01/2002 at 11:07 <br />Discard: 12/02/2002 <br />EFFL-W-021022 Grab Water <br />Facility## 95775 SIRC <br />301 Kettleman Lane -Lodi T0607700839 NA <br />0 <br />Page 1 of 1 <br />Account Number: 10869 <br />ChevronTexaco <br />6001 Bollinger Canyon Rd L4310 <br />San Ramon CA 94583 <br />KLEFF <br />As Received <br />CAT As Received Method Dilution <br />No. Analysis Name CAS Number Result Detection Unite Factor <br />Limit <br />01728 TPH-GPO - Waters n.a. N.D. 100. ug/1 1 <br />The reported concentration of TPH-GRO does not include MTBE or other <br />gasoline constituents eluting prior to the C6 (n -hexane) TPH-GRO range <br />start time. <br />A site-specific MSD sample was not submitted for the project. A LCS/LCSD <br />Was performed to demonstrate precision and accuracy at a batch level. <br />01412 Methanol and Ethanol <br />01414 <br />Methanol (by Direct Injection) 67-56-1 <br />N.D. <br />400. <br />ug/l <br />1 <br />599 <br />BTEX + oxygenates by 8260D <br />01587 <br />Ethanol 64-17-5 <br />N.D. <br />100- <br />ug/1 <br />1 <br />02010 <br />Methyl t -butyl ether 1634-04-4 <br />N.D. <br />2. <br />ug/l <br />1 <br />02011 <br />di -Isopropyl ether 108-20-3 <br />N.D- <br />2. <br />ug/l <br />1 <br />02013 <br />Ethyl t -butyl ether 637-92-3 <br />N.D. <br />2. <br />ug/1 <br />1 <br />02014 <br />t -Amyl methyl ether 994-05-8 <br />N.D. <br />2. <br />ug/1 <br />1 <br />02015 <br />t -Butyl alcohol 75-65-0 <br />N.D. <br />10. <br />ug/1 <br />1 <br />05401 <br />Benzene 71-43-2 <br />N.D. <br />2.. <br />ug/l <br />1 <br />05402 <br />1,2-Dichloroethane 107-06-2 <br />N.D. <br />2. <br />ug/l <br />1 <br />05407 <br />Toluene 108-88-3 <br />N.D. <br />2. <br />ug/l <br />1 <br />05412 <br />1,2-Dibromoethane 106-93-4 <br />N.D. <br />2. <br />u9/1 <br />1 <br />05415 <br />Ethylbenzene 100-41-4 <br />N.D. <br />2. <br />ug/l <br />1 <br />06310 <br />Xylene (Total) 1330-20-7 <br />N.D_ <br />2. <br />ug/l <br />1 <br />State of California Lab Certification No. 2116 <br />E <br />Laboratory <br />Chronicle <br />I4 CAT <br />Analysis <br />Dilution <br />No. <br />Analysis Name Method <br />Trial# <br />Date and Time Analyst <br />Factor <br />'E 01728 <br />TPH-GRO - Waters N. CA LUFT Gasoline <br />1 <br />10/26/2002 <br />17:41 K. Robert James <br />1 <br />Method <br />01412 <br />Methanol and Ethanol SW -846 8015E <br />1 <br />10/31/2002 <br />10:59 Lisa A Johnson <br />1 <br />01594 <br />BTEX + Oxygenates by 8260E SW -846 8260E <br />1 <br />10/29/2002 <br />00:29 David A <br />Hoppman <br />1 <br />01146 <br />GC VOA Water Prep SW -846 5030E <br />1 <br />10/26/2002 <br />17:41 K. Robert James <br />n.a. <br />` 01163 <br />GC/MS VOA Water Prep SW -846 5030B <br />1 <br />10/29/2002 <br />00:29 David A <br />Hoppman <br />n.a. <br />1 <br />Lancaster Laboratories, Inc. <br />MEMBER 2425 New Holland Pike <br />Box 12425 <br />®PO <br />Lancaster, PA 17605.2425 <br />717-656-2300 Fax: 717-656-2681 <br />2216 Rev. <br />9111100 <br />