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Lancaster <br />Laboratories <br />Lancaster Laboratories Sample No. WW 3950564 <br />Collected:11/20/2002 10:10 by ST <br />Submitted: 11/27/2002 09:40 <br />Reported: 12/12/2002 at 11:41 <br />Discard: 01/12/2003 <br />EFF -1-W-021120 Grab Water <br />Facility# 95775 SIRC <br />301 W Kettleman Ln Lodi 70607700839 EFF -1 <br />KLEFF <br />Page 1 of 2 <br />Account Number: 10869 <br />ChevronTexaco <br />6001 Bollinger Canyon Rd L4310 <br />San Ramon CA 94583 <br />As Received <br />CAT As Received Method <br />No. Analysis Name Dilution <br />CAS Number Result Detection Unita Factor <br />01728 TPH-GRO - WatersLimit <br />n.a. N.D. 100. ug/l 1 <br />The reported concentration of TPH-GRO does not include MTBE or other <br />gasoline constituents eluting prior to the C6 (n -hexane) TPH-GRO range <br />start time. <br />A site-specific MSD sample was not submitted for the project. A LCS/LCSD <br />was performed to demonstrate precision and accuracy at a batch level. <br />01412 Methanol and Ethanol <br />"-,01414 <br />[f <br />Methanol (by Direct Injection) <br />67-56-1 <br />N -D. <br />400. <br />ug/l 1 <br />_ JJ1594 <br />BTEX + Oxygenates by 8260B <br />01594 <br />BTEX i Oxygenates by 8260B <br />01146 <br />GC VOA Water Prep <br />01587 <br />Ethanol <br />64-17-5 <br />N.D. <br />100. <br />ug/1 1 <br />02010 <br />Methyl t -butyl ether <br />1634-04-4 <br />N.D. <br />2. <br />ug/l 1 <br />02011 <br />di -Isopropyl ether <br />108-20-3 <br />N.D: <br />2. <br />ug/1 1 <br />02013 <br />Ethyl t -butyl ether <br />637-92-3 <br />N.D. <br />2. <br />ug/1 1 <br />02014 <br />t -Amyl methyl ether <br />994-05-8 <br />N.D. <br />2. <br />ug/1 1 <br />02015 <br />t -Butyl alcohol <br />75-65-0 <br />N.D. <br />10. <br />ug/l, 1 <br />05401 <br />Benzene <br />71-43-2 <br />N.D_. <br />2. <br />ug/1 1 <br />05402 <br />1,2-Dichloroethane <br />107-06-2 <br />N.D. <br />2. <br />ug/1 1 <br />05407 <br />Toluene <br />108-88-3 <br />N.D. <br />2. <br />_ <br />ug/l 1 <br />05412 <br />1,2-Dibromoethane <br />106-93-4 <br />N.D. <br />2. <br />ug/1 1 <br />05415 <br />Ethylbenzene <br />100-41-4 <br />N.D. <br />2. <br />ug/l 1 <br />06310 <br />Xylene (Total) <br />1330-20-7 <br />N.D. <br />2 <br />ug/l 1 <br />State of California Lab Certification No. 2116 <br />CAT <br />No. <br />Analysis Name <br />01728 <br />TPH-GRO - Waters <br />01412 <br />Methanol and Ethanol <br />01594 <br />BTEX i Oxygenates by 8260B <br />01146 <br />GC VOA Water Prep <br />63 <br />GC/MS VOA Water Prep <br />Laboratory Chronicle <br />Lancaster laboratories, inc. <br />M B M B E R 2425 New Holland Pike <br />La Box 12425 <br />Lancaster, PA 17605-2425 <br />717-656-2300 Fax: 717-656-2681 <br />Dilution <br />Analysis <br />Method <br />Factor <br />Trial; <br />Date and <br />Time <br />N. CA LUFT Gasoline <br />1 <br />11/29/2002 <br />20:44 <br />Method <br />Melissa <br />D Mann <br />n.a. <br />Kenneth <br />SW -846 <br />8015B <br />1 <br />12/02/2002 <br />21:22 <br />SW -846 <br />8260B <br />1 <br />12/02/2002 <br />11:29 <br />SW -846 <br />5030B <br />1 <br />11/29/2002 <br />20:44 <br />SW -846-5030B <br />1 <br />12/02/2002 <br />11:29 <br />Lancaster laboratories, inc. <br />M B M B E R 2425 New Holland Pike <br />La Box 12425 <br />Lancaster, PA 17605-2425 <br />717-656-2300 Fax: 717-656-2681 <br />2216 Rev. 10/2/02 <br />Dilution <br />Analyst <br />Factor <br />Melissa <br />D Mann <br />1 <br />Lisa A Johnson <br />1 <br />Kenneth <br />L Baley Jr <br />1 <br />Melissa <br />D Mann <br />n.a. <br />Kenneth <br />L Boley Jr <br />n.a. <br />2216 Rev. 10/2/02 <br />