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Lancaster <br />Laboratories <br />Page 1 of I <br />Lancaster Laboratories Sample No. WW 3965838 <br />Collected:12/17/2002 11:30 by ST <br />Submitted: 12/19/2002 14:35 <br />Reported: 12/31/2002 at 20:42 <br />Discard: 01/31/2003 <br />EFFL-W-021217 Grab Water <br />Facility# 95775 SIRC <br />301 W Kettleman-Lodi T0607700839 NA <br />WKLEF <br />Account Number: 10869 <br />ChevronTexaco <br />6001 Bollinger Canyon Rd L4310 <br />San Ramon CA 94583 <br />Lancaster Laboratories, Inc. <br />U E M B E R 2425 New Rolland Pike <br />®PO Box 12425 <br />Lancaster, PA 17605-2425 <br />717-656-2300 Fax: 717-656-2681 <br />2216 Rev. 10/2/02 <br />As Received <br />CAT <br />As Received Method <br />Dilution <br />No. <br />Analysis Name <br />CAS Number <br />Result <br />Detection <br />Units Factor <br />Limit <br />01728 <br />TPH-GRO - Waters <br />n.a_ <br />N.D_ <br />50. <br />ug/l <br />1 <br />The reported concentration <br />of TPH-GRO does not <br />include MTBE or other <br />gasoline constituents eluting prior to the C6 <br />(n -hexane) <br />TPH-GAO range <br />start time. <br />A site-specific MSD sample <br />was not submitted for <br />the project. A LCS/LCSD <br />was performed to demonstrate precision and accuracy <br />at a <br />batch level. <br />01412 <br />Methanol and Ethanol <br />01414 <br />Methanol (by Direct Injection) <br />67-56-1 <br />N.D. <br />400. <br />ug/l <br />1 <br />1594 <br />BTEX + Oxygenates by 8260B <br />01587 <br />Ethanol <br />64-17-5 <br />N.D. <br />100. <br />ug/l <br />1 <br />02010 <br />Methyl t -butyl ether <br />1634-04-4 <br />N.D. <br />2. <br />ug/l <br />1 <br />02011 <br />di-leopropyl ether <br />108-20-3 <br />N.D. <br />2. <br />ug/l <br />1 <br />02013 <br />Ethyl t -butyl ether <br />637-92-3 <br />N.D_ <br />2_ <br />ug/l <br />i <br />02014 <br />t -Amyl methyl ether <br />994-05-8 <br />N.D. <br />2. <br />ug/l <br />1 <br />02015 <br />t -Butyl alcohol <br />75-65-0 <br />N.D. <br />10. <br />ug/1 <br />1 <br />05401 <br />Benzene <br />71-43-2 <br />N.D. <br />2. <br />ug/l <br />1 <br />05402 <br />1,2-Dichloroethane <br />107-06-2 <br />N.D. <br />2. <br />ug/l <br />1 <br />05407 <br />Toluene <br />108-88-3 <br />N.D. <br />2. <br />ug/l <br />1 <br />05412 <br />1,2-Dibromoethane <br />106-93-4 <br />N.D. <br />2- <br />ug/1 <br />1 <br />05415 <br />Ethylbenzene <br />100-41-4 <br />N.D. <br />2. <br />ug/1 <br />1 <br />06310 <br />Xylene (Total) <br />1330-20-7 <br />N.D. <br />2. <br />ug/l <br />1 <br />State of California Lab Certification No. 2116 <br />Laboratory <br />Chronicle <br />CAT <br />Analysia <br />Dilution <br />No. <br />Analysis Name <br />Method <br />Trial# <br />Date and Time <br />Analyst <br />Factor <br />01728 <br />TPH-GRO - Waters <br />N. CA LUFT Gasoline 1 <br />12/20/2002 20:31 <br />Martha L <br />Seidel <br />1 <br />Method <br />01412 <br />Methanol and Ethanol <br />SW -846 8015B <br />1 <br />12/30/2002 17:32 <br />Lisa A Johnson <br />1 <br />01594 <br />BTEX + Oxygenates by 826QB <br />SW -846 8260B <br />1 <br />12/26/2002 19:59 <br />Susan McMahon-Luu <br />1 <br />01146 <br />GC VOA Water Prep <br />SW -846 5030B <br />1 <br />12/20/2002 20:31 <br />Martha L <br />Seidel <br />n.a. <br />01163 <br />GC/MS VOA Water Prep <br />SW -846 5030E <br />1 <br />12/26/2002 19:59 <br />Susan McMahon-Luu <br />n_a. <br />Lancaster Laboratories, Inc. <br />U E M B E R 2425 New Rolland Pike <br />®PO Box 12425 <br />Lancaster, PA 17605-2425 <br />717-656-2300 Fax: 717-656-2681 <br />2216 Rev. 10/2/02 <br />