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Lancaster Laboratories <br />Where quality rs a science. <br />Page l of i <br />Lancaster Laboratories Sample No. WW 3933170 <br />Collected:10/29/2002 11:00 by TC Account Number: 10906 <br />I <br />Submitted: 11/04/2002 08:35 ChevronTexaco <br />Reported: 11/14/2002'at 19:586001 Bollinger Canyon Rd L4310 <br />Discard: 12/15/2002 San Ramon CA 94583 <br />EX -3-W-021029, Grab Water , <br />Facility# 95775 Job# 386408 GRD <br />301 W Kettleman Ln -Lodi T0607700839 EX -3 <br />L"IN a 161 <br />Lancaster Laboratories, Inc. <br />M E M B E R 2425 New Holland Pike <br />PO Box 12425 <br />Lancaster, PA 17605-2425 <br />717-656-2300 Fax: 717-656-2681 <br />2216 Rev. 9111/00 <br />As Received <br />CAT <br />As Received Method - <br />Dilution <br />No. <br />Analysis Name <br />CAS Number <br />Result <br />Detection <br />Units <br />Factor <br />Limit <br />01728 <br />TPH-GRO - Waters <br />n.a. <br />N.D. <br />50. <br />ug/1 <br />1 <br />The reported concentration <br />of TPH-GRO does not <br />include MTBE or other <br />gasoline constituents eluting prior to the C6 <br />(n -hexane) <br />TPH-GRO range <br />y <br />start time. <br />A site-specific MSD sample <br />was not submitted for the project. A LCS/LCSD <br />was performed to demonstrate precision and accuracy at a <br />batch level. <br />h <br />01412 <br />Methanol and Ethanol <br />1414 <br />Methanol (by Direct Injection) 67-56-1 <br />N.D. <br />200. <br />ug/l <br />1 <br />01594 <br />BTEX + Oxygenates by 8260B <br />01587 <br />Ethanol <br />64-17-5 <br />N.D. <br />50. <br />ug/1 <br />1 <br />02010 <br />Methyl t -butyl ether <br />1634-04-4 <br />21. <br />0.5 <br />ug/l <br />1 <br />02011 <br />di -Isopropyl ether <br />108-20-3 <br />N.D. <br />0.5 <br />ug/1 <br />1 <br />02013 <br />Ethyl t -butyl ether <br />637-92-3 <br />2. <br />0.5 <br />ug/l <br />1 <br />02014 <br />t -Amyl methyl ether <br />994-05-8 <br />N.D. <br />0-5 <br />ug/l <br />1 <br />02015 <br />t -Butyl alcohol <br />75-65-0 <br />N.D. <br />S. <br />ug/1'' <br />1 <br />05401 <br />Benzene <br />71-43-2 <br />N.D. <br />0.5 <br />ug/l <br />1 , <br />05402 <br />1,2-Dichloroethane <br />107-06-2 <br />N.D. <br />0,5 <br />ug/l <br />1 <br />05407 <br />Toluene <br />108-88-3, <br />N_D. <br />0.5 <br />ug/l <br />1- <br />05412 <br />1,2-Dibromoethane <br />106-93-4 <br />N.D. <br />0.5 <br />ug/l <br />1 <br />05415 <br />Ethylbenzene <br />100-41-4 _ <br />N.D. <br />0.5 <br />ug/1 <br />1 <br />06310 <br />Xylene -(Total) <br />1330-20-7 <br />N.D.; <br />0.5 <br />ug/l <br />1 <br />State of California Lab Certification <br />No. 2116 <br />F <br />r <br />Laboratory <br />Chronicle <br />CAT <br />Analysis <br />Dilution <br />No. <br />Analysis Name <br />Method <br />Trial# <br />Date and Time. <br />Analyst <br />Factor <br />01728 <br />TPH-GRO - Waters <br />N. CA LUFT Gasoline 1 <br />11/05/2002 15:01 <br />Melissa D <br />Mann <br />1 <br />Method <br />01412 <br />Methanol and Ethanol <br />SW -846 8015E <br />1 <br />11/07/2002 19:42 <br />Lisa A Johnson <br />1 <br />01594 <br />BTE% + Oxygenates by 8260B <br />SW -846 8260E <br />1 <br />11/07/2002 03:38 <br />Kenneth L <br />Boley Jr <br />1 <br />01146 <br />GC VOA Water Prep <br />SW -846 5030B <br />1 <br />11/05/2002 15:01 <br />Melissa D <br />Mann <br />n.a: <br />(-41,163 <br />GC/MS VOA Water Prep <br />SW -846 5030E F <br />1 <br />11/07/2002 03:38 <br />Kenneth L <br />Boley Jr <br />n.a... <br />Lancaster Laboratories, Inc. <br />M E M B E R 2425 New Holland Pike <br />PO Box 12425 <br />Lancaster, PA 17605-2425 <br />717-656-2300 Fax: 717-656-2681 <br />2216 Rev. 9111/00 <br />