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r <br />4207724 <br />103 <br />106 <br />102 <br />103 <br />4207725 <br />104 <br />105 <br />102 <br />Lancaster <br />4207726 <br />103 <br />105 <br />Laboratories <br />103 <br />Analysis Report <br />4207727 <br />2425 New Holland Pike, PO Box 12425, Lancaster, PA 17605-2425 •717-656-2300 Fax 717-656-2681 • www.lancasterlabs.com <br />105 <br />103 <br />103 <br />4207728 <br />Page 7 of 8 <br />105 <br />Quality Control Summary <br />103 <br />`- <br />Client Name: ChevronTexaco <br />104 <br />Group Number: 883197 <br />103 <br />102 <br />Reported: 02/12/04 at 08:28 <br />AM <br />103 <br />105 <br />103 <br />103 <br />Surrogate <br />Quality Control <br />104 <br />--. <br />4207700 95 <br />94 <br />96 <br />Ms <br />104 <br />4207701 96 <br />96 <br />95 <br />93 <br />MSD <br />4207702 96 <br />95 <br />95 <br />93 <br />94 <br />177 <br />4207703 96 <br />96 <br />96 <br />85-112 <br />83-113 <br />4207704 95 <br />95 <br />96 <br />93 <br />93 <br />4207705 96 <br />96 <br />96 <br />92 <br />4207706 96 <br />96 <br />95 <br />95 <br />4207707 96 <br />96 <br />95 <br />94 <br />4207708 96 <br />96 <br />95 <br />93 <br />Blank 96 <br />96 <br />95 <br />92 <br />LCS 96 <br />95 <br />96 <br />95 <br />Ms 97 <br />96 <br />95 <br />94 <br />MSD 96 <br />97 <br />96 <br />95 <br />Limits: 81-120 <br />82-112 <br />85-112 <br />83-113 <br />Analysis Name: BTEX+5 Oxygenatea+EDC+EDB+ETOH <br />Batch number: P040391AA <br />Dibromofluoromethane <br />1,2-Dichloroethane-d4 <br />Toluene -d8 <br />4-Bromofluorobenzene. <br />4207709 96 <br />96 <br />95 <br />93 <br />4207710 96 <br />94 <br />95 <br />93 <br />4207711 96 <br />94 <br />94 <br />93 <br />9207712 96 <br />95 <br />94 <br />93 <br />[^ <br />4207713 96 <br />96 <br />94 <br />93 <br />FE4 <br />4207714 95 <br />95 <br />94 <br />92 <br />4207715 97 <br />95 <br />94 <br />93 <br />4207716 97 <br />96 <br />95 <br />93 <br />4207717 97 <br />96 <br />94 <br />93 <br />4207716 96 <br />96 <br />94 <br />93 <br />4207719 96 <br />96 <br />94 <br />93 <br />4207722 95 <br />95 <br />95 <br />93 <br />4207723 97 <br />95 <br />95 <br />93 <br />Blank 96 <br />95 <br />95 <br />93 <br />LCS 98 <br />96 <br />95 <br />94 <br />MS 96 <br />93 <br />94 <br />99 <br />MSR 96 <br />99 <br />94 <br />96 <br />Limits: 81-120 <br />82-112 <br />85-112 <br />83-113 <br />Analysis Name: BTEX+5 Oxygenates+EDC+EDB+ETOH <br />Batch number: P040392AA <br />,. <br />Dibromofluoromethane <br />1,2-Dichloroethane-d4 <br />Toluene -d8 <br />4-Bromofluorobenzene <br />*- Outside of specification <br />(1) The result for one or both determinations was less than five times the LOQ. <br />(2) The background result was more than four times the spike added. <br />4207724 <br />103 <br />106 <br />102 <br />103 <br />4207725 <br />104 <br />105 <br />102 <br />103 <br />4207726 <br />103 <br />105 <br />102 <br />103 <br />4207727 <br />103 <br />105 <br />103 <br />103 <br />4207728 <br />103 <br />105 <br />103 <br />103 <br />4207729 <br />104 <br />106 <br />103 <br />102 <br />Blank <br />103 <br />105 <br />103 <br />103 <br />LCS <br />104 <br />105 <br />103 <br />103 <br />Ms <br />104 <br />105 <br />102 <br />103 <br />- <br />MSD <br />102 <br />104 <br />103 <br />104 <br />Limits. <br />Analysis <br />81-120 <br />Name: BTEX+5 <br />82-112 <br />Oxygenates+EDC+EDB+ETOH <br />85-112 <br />83-113 <br />*- Outside of specification <br />(1) The result for one or both determinations was less than five times the LOQ. <br />(2) The background result was more than four times the spike added. <br />