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ik <br />rn <br />er <br />*L�abo�ratories <br />Quality Control Summary <br />Client Name ChevronTexaco <br />Reported 12/12/02 at 11 42 AM <br />3950562 <br />102 <br />3950563 <br />97 <br />3950564 <br />104 <br />3950565 <br />102 <br />3950566 <br />102 <br />Blank <br />105 <br />LCS <br />105 <br />LCSD <br />105 <br />MS <br />101 <br />Limits S'1 -14b <br />Analysis Name Methanol and Ethanol <br />Batch number 023360042A <br />Acetone <br />Group Number 832605 <br />Surrogate Quality Control <br />Page 3 of 4 <br />3950561 <br />104 <br />3950562 <br />102 <br />3950563 <br />101 <br />3950564 <br />104 <br />3950565 <br />100 <br />Blank <br />104 <br />LCS <br />103 <br />MS <br />102 <br />MSD <br />98 <br />imits 72-128 <br />Analysis Name BTEX + Oxygenates <br />by <br />8260B <br />Batch number N023341AB <br />Dibromofluoromethane <br />1,2-Dichloroethane-d4 <br />Toluene -d8 <br />4-Bromofluorobenzene <br />3950565 92 <br />97 <br />97 <br />94 <br />3950566 92 <br />95 <br />97 <br />93 <br />Blank 93 <br />95 <br />96 <br />94 <br />LCS 93 <br />97 <br />103 <br />103 <br />MS 93 <br />99 <br />103 <br />103 <br />MSD 93 <br />99 <br />103 <br />104 <br />Limits 86-118 <br />80-120 <br />88-110 <br />86-115 <br />Analysis Name BTEX + Oxygenates <br />by <br />8260E <br />Batch number X023361AA <br />Dibromofluoromethane <br />1,2-Dichloroethane-d4 <br />Toluene -d8 <br />4-Bromofluorobenzene <br />3950562 94 <br />95 <br />96 <br />92 <br />3950563 93 <br />96 <br />97 <br />94 <br />3950564 93 <br />96 <br />97 <br />94 <br />Blank 93 <br />95 <br />96 <br />94 <br />LCS 91 <br />97 <br />101 <br />101 <br />MS 90 <br />94 <br />101 <br />102 <br />MSD 91 <br />95 <br />101 <br />101 <br />Limits 86-118 <br />84-120 <br />88-110 <br />86-115 <br />Analysis Name BTEX + Oxygenates <br />by <br />6260B <br />Batch number N023361AB <br />Dibromofluoromethane <br />1,2-Dichloroethane-d4 <br />Toluene -d8 <br />4-Bromofluorobenzene <br />*- Outside of specification <br />(1) The result for one or both determinations was less than five times the LOQ <br />0) The background result was more than four times the spike added <br />Lancaster Laboratories Inc <br />M EM BE R 2425 New Holland Pike <br />La Box 1 <br />Lancaster <br />PA PA 77605-2425 <br />717 656-2300 fax 717-656 2681 <br />2216 Rev 10/2102 <br />