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Lancaster Laboratories 1 ; <br />Wh&2 ya mol Summary J � <br />Client Name ChevronTexaco <br />MSD <br />MS/MSD <br />Group <br />Number <br />819138 <br />Reported 09/11/02 at 06 <br />10 PM <br />RPD <br />MAX Cone <br />Sample <br />number(s) <br />3880016-3880020 <br />Laboratory <br />Compliance Quality <br />58-137 <br />Control <br />20 <br />Blank <br />Blank <br />Report LCS <br />LCSD <br />LCS/LCSD <br />Analysis Name <br />Result <br />MDL <br />Units <br />%REC <br />%REC <br />Limits <br />Batch number 022280004A <br />sample <br />number(s) <br />3880016-3880020 <br />10 <br />30 <br />103 <br />Methanol (by Direct ln)ection) <br />N D <br />200 <br />ug/l <br />92 <br />105 <br />64-130 <br />Batch number 02228A56A <br />Sample <br />number(s) <br />3880016-3880021 <br />73-123 <br />2 <br />30 <br />TPH-GRO - Waters <br />N D <br />So <br />ug/l <br />90 <br />90 <br />74-116 <br />Batch number N022222AA <br />Sample <br />number(s) <br />3880016-3880020 <br />104 <br />78-134 <br />2 <br />Ethanol <br />N D <br />50 <br />ug/l <br />102 <br />30 <br />43-159 <br />Methyl t -butyl ether <br />N D <br />5 <br />ug/l <br />101 <br />99 <br />77-127 <br />dl -Isopropyl ether <br />N D <br />5 <br />ug/l <br />104 <br />2 <br />74-125 <br />Ethyl t -butyl ether <br />N D <br />5 <br />ug/l <br />95 <br />74-120 <br />t -Amyl methyl ether <br />N D <br />5 <br />ug/l <br />95 <br />71-1,14 <br />t -Butyl alcohol <br />N D <br />5 <br />ug/l <br />95 <br />59-139 <br />Benzene <br />N D <br />5 <br />ug/l <br />103 <br />85-117 <br />1,2-Dichloroethane <br />N D <br />5 <br />ug/l <br />101 <br />77-132 <br />Toluene <br />N D <br />5 <br />ug/l <br />105 <br />85-115 <br />1,2-Dlbromoethane <br />N D <br />5 <br />u9/1 <br />100 <br />81-114 <br />Ethylbenzene <br />N D <br />5 <br />ug/l <br />104 <br />82-119 <br />Xylene (Total) <br />N D <br />5 <br />ug/l <br />105 <br />84-120 <br />• <br />Analysis Name <br />Batch number 022280004A <br />Methanol (by Direct Infection) <br />Batch number 0222BA56A <br />TPH-GRD - Waters <br />Batch number N022282AA <br />Ethanol <br />Methyl t -butyl ether <br />di -Isopropyl ether <br />Ethyl t -butyl ether <br />t -Amyl methyl ether <br />t -Butyl alcohol <br />Benzene <br />1,2-Dachloroethane <br />Toluene <br />1,2-Dibromoethane <br />Ethylbenzene <br />Xylene (Total) <br />Sample Matrix Quality Control <br />MS <br />MSD <br />MS/MSD <br />RPD BKG <br />%REC <br />%REC <br />Limits <br />RPD <br />MAX Cone <br />Sample <br />number(s) <br />3880016-3880020 <br />92 <br />92 <br />58-137 <br />0 <br />20 <br />Sample <br />number(s) <br />3880016-3880021 <br />99 <br />74-132 <br />Sample <br />number(s) <br />3880016-3880020 <br />101 <br />111 <br />34-163 <br />10 <br />30 <br />103 <br />103 <br />69-134 <br />0 <br />30 <br />107 <br />105 <br />68-133 <br />2 <br />30 <br />94 <br />96 <br />73-123 <br />2 <br />30 <br />95 <br />95 <br />69-118 <br />0 <br />30 <br />97 <br />96 <br />51-148 <br />1 <br />30 <br />106 <br />104 <br />78-134 <br />2 <br />30 <br />110 <br />108 <br />73-136 <br />2 <br />30 <br />105 <br />105 <br />83-127 <br />0 <br />30 <br />99 <br />99 <br />78-120 <br />0 <br />30 <br />107 <br />105 <br />82-134 <br />2 <br />30 <br />108 <br />107 <br />82-130 <br />1 <br />30 <br />*- Outside of specification <br />(1) The result for one or both determinations was less than five times the LOQ <br />0The background result was more than four times the spike added <br />Lancaster Laboratories Inc <br />MEMBER 2425 New Holland Pike <br />®PO Box 12425 <br />Lancaster PA 176052425 <br />717 656 2300 Fax 71717656 2681 <br />Page I of 3 <br />RPD RPD Max <br />0 <br />DUP DUP <br />Cone RPD <br />30 <br />Dup <br />RPD <br />Max <br />2216 Rev 9111100 <br />