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Lancaster Laboratories Page 2 of 3 <br />MQuqJAtpyaQgmtwo1 Summary <br />Client Mame ChevronTexaco Group Number 820956 <br />Reported 09/11/02 at 06 20 PM <br />Surrogate Quality Control <br />Analysis Name TPH-GRO _ Waters <br />Batch number 02246A56A <br />Trlfluorotoluene-F <br />3888953 86 <br />3888954 85 <br />3888955 87 <br />3888956 87 <br />3BB8957 84 <br />3888958 86 <br />Blank 87 <br />LCs 96 <br />LCSD 97 <br />MS 97 <br />MSD 96 <br />Limits 57-146 <br />Analysis Name Methanol and Ethanol <br />Batch number 022480008A <br />Acetone <br />8953 99 <br />3888954 106 <br />3888955 104 <br />3888956 103 <br />3688957 108 <br />Blank 104 <br />LCS 104 <br />MS 98 <br />MSD 103 <br />Limits 72-128 <br />Analysis Name BTEX + Oxygenates by <br />8260B <br />Batch number N022471AA <br />Dibromofluoromethane <br />1,2-Dichlorcethane-d4 <br />Toluene -d8 <br />4-Bromofluorobenzene <br />3888953 97 <br />93 <br />97 <br />93 <br />3888954 99 <br />95 <br />98 <br />93 <br />3888955 100 <br />95 <br />98 <br />94 <br />3888956 100 <br />95 <br />97 <br />94 <br />3888957 101 <br />97 <br />97 <br />93 <br />Blank 98 <br />94 <br />98 <br />93 <br />LCS 96 <br />95 <br />100 <br />100 <br />MS 96 <br />93 <br />99 <br />99 <br />MSD 95 <br />93 <br />100 <br />99 <br />*- Outside of specification <br />(1) The result for one or both determinations was less than five times the LOQ <br />0The background result was more than four times the spike added <br />Lancaster Laboratories Inc <br />M E M B E R 2425 New Holland Pike <br />PO Box 12425 <br />WANLancaster PA 17605 2425 <br />717 656 2300 fax 717 656 2681 2216 Rev 9111/00 <br />