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s Ana e�pa <br />a; ESO Bas :124215 haasCer PA :17605-242b 717 656-29Q0 :Fao....... <br />i:797 65'0 2881 . VrWwAarrocasl i[ab&:corn <br />*- Outside of specification <br />(1) The result for one or both determinations was less than five times the LUQ, <br />?) The background result was more than four times the spike added. <br />Page E of 3 <br />Quality <br />Control Summary <br />Client Name: ChevronTexaco <br />Group Number: <br />849104 <br />Reported: 05/05/03 at 08:56 AM <br />Laboratory <br />Compliance Quality <br />Control <br />Blank <br />Blank Report LCS LCSD <br />LCS/LCSD <br />Analysis Name <br />Result <br />MDL Unita REC $RSC <br />Limits <br />RPD RPD Max <br />Batch number; 03112A07D <br />Sample <br />number(s). 4031022-4031025 <br />TPH-GRO - Waters <br />N.D. <br />50. ug/l 109 <br />70-130 <br />Batch number: 03113AO7A <br />Sample <br />number(s): 4031026 <br />TPH-GRO - Waters <br />N.D. <br />50. ug/l 92 <br />70-130 <br />Batch number: 031140019A <br />Sample <br />number(s): 4031022-4031025 <br />Methanol (by Direct. Injection) <br />N.D. <br />200, ug/l 96 <br />78-114 <br />Batch number: P031122AA <br />Sample <br />number(s): 4031022-4031026 <br />Ethanol <br />N.D_ <br />50. u9/1 113 <br />43-1.59 <br />Methyl Tertiary Butyl Ether <br />N.D. <br />.5 ug/l 100 <br />77-127 <br />di -isopropyl ether <br />N.D. <br />.5 ug/l 99 <br />74=125 <br />Ethyl t -butyl ether <br />N.D. <br />.5 u9/1 100 <br />74-120 <br />t -Amyl methyl ether <br />N.D_ <br />.5 ug/l 99 <br />79-11.3 <br />t -Butyl alcohol <br />N.D. <br />5. ug/l 106 <br />53-147 <br />Benzene <br />N.D. <br />.5 ug/1 102 <br />85-117 <br />1,2-Dichloroethane <br />N.D. <br />.5 ug/l 99 <br />77-132 <br />Toluene <br />N,D. <br />.5 ug/1 101 <br />85-115 <br />1,2-Dibromoethane <br />N.D. <br />.5 ug/1 98 <br />81-114 <br />Ethylbenzene <br />N -D. <br />.5 ug/l 99 <br />82-119 <br />ylene (Total) <br />N.D. <br />.5 ug/1 99 <br />84-120 <br />Sample Matrix Quality Control <br />MS <br />MSD MS/MSA RPD BKG <br />DT3P <br />DUP Dup <br />RPD <br />Analysis Name <br />$REC <br />%REC Limits RPD MAX Conc <br />Cone <br />RPD Max <br />Batch number: 03112A07D <br />Sample <br />number(s): 4031022-4031025 <br />TPH-GRO - Waters <br />115 <br />105 70-130 8 30 <br />Batch number: 03113AO7A <br />Sample <br />number(s): 4031026 <br />TPH-GRO - Waters <br />107 <br />108 70-130 1 30 <br />Batch number; 031140019A <br />Sample <br />number(s): 4031022-4031025 <br />Methanol (by Direct injection) <br />92 <br />92 78-116 0 20 <br />Batch number: P031122AA <br />Sample <br />number(s); 4031022-4031026 <br />Ethanol <br />126 <br />133 34-163 5 30 <br />Methyl Tertiary Butyl Ether <br />105 <br />107 69-134 1 30 <br />di -Isopropyl ether <br />105 <br />107 75-130 2 30 <br />Ethyl t -butyl, ether <br />105 <br />105 73-123 0 30 <br />t -Amyl methyl ether <br />106 <br />108 77-117 2 30 <br />t -Butyl alcohol <br />113 <br />116 39-155 2 30 <br />Benzene <br />112 <br />112 83-126 1 30 <br />1,2-Dichloroethane <br />105 <br />106 73-136 1 30 <br />Toluene <br />108 <br />109 83-127 2 30 <br />1,2-Dibromoethane <br />100 <br />103 78-120 3 30 <br />Ethylbenzene <br />105 <br />109 82-134 4 30 <br />Xylene (Total) <br />106 <br />109 82-130 3 30 <br />*- Outside of specification <br />(1) The result for one or both determinations was less than five times the LUQ, <br />?) The background result was more than four times the spike added. <br />