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Batch number: 022280004A <br />Methanol (by Direct Injection) <br />Batch number: 0222BA56A <br />TPH-GRO - Waters <br />Batch number: N022282AA <br />Ethanol <br />Methyl t -butyl ether <br />di -Isopropyl ether <br />Ethyl t -butyl ether <br />t -Amyl methyl ether <br />t -Butyl alcohol <br />Benzene <br />1,2-Dichloroeth—e <br />Toluene <br />1,2-Dibromoethane <br />Ethylbenzene <br />Xylene (Total) <br />Sample <br />number(s): 3880016-3880020 <br />92 <br />92 <br />58-137 <br />0 <br />20 <br />Sample <br />number(s): 3880016-3880021 <br />Lancaster <br />99 <br />Laboratories <br />Sample <br />number(s): 3880016-3880020 <br />Page 1 of 3 <br />111 <br />34-163 <br />10 <br />30 <br />103 <br />103 <br />69-134 <br />0 <br />30 <br />v..�. <br />=i <br />T <br />68-133 <br />WheQ <br />,��Va�'o7. <br />94 <br />Summary <br />�. <br />F <br />, p`+� <br />30 <br />Client Name: ChevronTexaco <br />95 <br />69-118 <br />0 <br />Group Number: <br />819138 <br />96 <br />Reported: 09/11/02 <br />at 06:1.0 PM <br />30 <br />106 <br />104 <br />78-134 <br />2 <br />30 <br />Laboratory Compliance <br />Quality <br />Control <br />2 <br />30 <br />Blank <br />Blank <br />Report <br />LCS LCSA <br />LCS/LCSD <br />99 <br />Analysis Name <br />Result <br />MDL <br />Units <br />%REC %REC <br />Limits <br />RPD RPD Max <br />Batch number: 022280004A <br />Sample <br />number(s) <br />3880016-3880020 <br />82-130 <br />1 <br />Methanol (by Direct Injection) <br />N.D. <br />200. <br />ug/l <br />92 <br />64-130 <br />Batch number: 0222BA56A <br />Sample <br />number(s): <br />3880016-3880021 <br />TPH-GRO - Waters <br />N.D. <br />50. <br />ug/l <br />90 90 <br />74-116 <br />0 30 <br />Batch number: N022282AA <br />Sample <br />number(s) <br />3880016-3880020 <br />Ethanol <br />N.D. <br />50. <br />ug/l <br />102 <br />43-159 <br />Methyl t -butyl ether <br />N.D. <br />.5 <br />ug/l <br />101 <br />77-127 <br />di -Isopropyl ether <br />N.D. <br />.5 <br />ug/l <br />104 <br />74-125 <br />Ethyl t -butyl ether <br />N.D. <br />5 <br />ug/1 <br />95 <br />74-120 <br />t -Amyl methyl ether <br />N.D. <br />.5 <br />ug/l <br />95 <br />71-114 <br />t -Butyl alcohol <br />N.D. <br />5. <br />ug/l <br />95 <br />59-139 <br />Benzene <br />N.D. <br />.5 <br />ug/l <br />103 <br />85-117 <br />1,2-Dichloroethane <br />N.D. <br />.5 <br />ug/l <br />101 <br />77--132 <br />Toluene <br />N.D. <br />_5 <br />ug/l <br />105 <br />85--115 <br />1,2-Dibromoethane <br />N.D. <br />.5 <br />ug/l <br />100 <br />81-114 <br />Ethylbenzene <br />N.D. <br />.5 <br />ug/1 <br />104 <br />82-119 <br />Xylene (Total) <br />N.D. <br />.5 <br />ug/l <br />105 <br />84-120 <br />40 <br />Sample <br />Matrix <br />Control <br />Quality <br />MS <br />MSD MS/MSB <br />RPD BKG <br />DUP <br />DUP PUP <br />RPA <br />Analysis Name <br />%RPC <br />%REC Limits RPD MAX Conc <br />Conc <br />RPD Max <br />Batch number: 022280004A <br />Methanol (by Direct Injection) <br />Batch number: 0222BA56A <br />TPH-GRO - Waters <br />Batch number: N022282AA <br />Ethanol <br />Methyl t -butyl ether <br />di -Isopropyl ether <br />Ethyl t -butyl ether <br />t -Amyl methyl ether <br />t -Butyl alcohol <br />Benzene <br />1,2-Dichloroeth—e <br />Toluene <br />1,2-Dibromoethane <br />Ethylbenzene <br />Xylene (Total) <br />Sample <br />number(s): 3880016-3880020 <br />92 <br />92 <br />58-137 <br />0 <br />20 <br />Sample <br />number(s): 3880016-3880021 <br />99 <br />74-132 <br />Sample <br />number(s): 3880016-3880020 <br />101 <br />111 <br />34-163 <br />10 <br />30 <br />103 <br />103 <br />69-134 <br />0 <br />30 <br />107 <br />105 <br />68-133 <br />2 <br />30 <br />94 <br />96 <br />73-123 <br />2 <br />30 <br />95 <br />95 <br />69-118 <br />0 <br />30 <br />97 <br />96 <br />51-148 <br />1 <br />30 <br />106 <br />104 <br />78-134 <br />2 <br />30 <br />110 <br />108 <br />73-136 <br />2 <br />30 <br />105 <br />105 <br />83-127 <br />0 <br />30 <br />99 <br />99 <br />78-120 <br />0 <br />30 <br />107 <br />105 <br />82-134 <br />2 <br />30 <br />108 <br />107 <br />82-130 <br />1 <br />30 <br />*- Outside of specification <br />(1) The result for one or both determinations was less than five times the LOQ. <br />The background result was more than four times the spike added. <br />Lancaster Laboratories, Inc. <br />M E M B E F:l 2425 New Holland Pike <br />®PO Bax 12425 <br />Lancaster, PA 17605-2425 <br />717.656.2300 Fax; 717-656.2681 <br />2216 Rev. 9/11too <br />