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Lancaster Laboratories <br />Where quality is a science. <br />Quality Control Summary <br />Client Name: ChevronTexaco <br />Reported: 09/27/02 at 01:13 PM <br />LCSD 93 <br />MS 94 <br />Limits: 57-146 <br />Analysis Name: Methanol and Ethanol <br />Batch number: 022630004A <br />Acetone <br />Group Number: 822883 <br />Surrogate Quality Control <br />Page 3 of 3 <br />3898975 <br />126 <br />3898976 <br />130* <br />3890977 <br />128 <br />3898978 <br />115 <br />3898979 <br />118 <br />Blank <br />104 <br />LCS <br />101 <br />MS <br />104 <br />MSD <br />104 <br />Limits: 72-128 <br />80-120 <br />88-110 <br />86-115 <br />Analysis Name: BTEX + oxygenates by <br />82608 <br />Batch number: N022592AB <br />Dibromofluoromethane <br />1,2-Dichloroethane-d4 <br />Toluene -de <br />4-Bromofluorobenzene <br />98975 96 <br />93 <br />93 <br />89 <br />98976 95 <br />91 <br />94 <br />89 <br />98977 95 <br />93 <br />93 <br />88 <br />898978 95 <br />91 <br />94 <br />89 <br />3898979 95 <br />93 <br />94 <br />89 <br />3898980 96 <br />92 <br />93 <br />89 <br />Blank 95 <br />91 <br />93 <br />88 <br />LCS 94 <br />93 <br />95 <br />91 <br />MS 95 <br />92 <br />95 <br />90 <br />MSD 95 <br />90 <br />94 <br />91 <br />Limits: 86-118 <br />80-120 <br />88-110 <br />86-115 <br />Analysis Name: BTEX + Oxygenates by <br />8260B <br />Batch number: N022601AA <br />Dibromofluoromethane <br />1,2-Dichloroethane-d4 <br />Toluene -d8 <br />4-Bromofluorobenzene <br />3898981 95 <br />93 <br />93 <br />89 <br />Blank 95 <br />91 <br />93 <br />88 <br />LCS 94 <br />91 <br />94 <br />91 <br />MS 95 <br />90 <br />94 <br />90 <br />MSD 95 <br />91 <br />94 <br />91 <br />Limits: 86-118 80-120 88-110 86-115 <br />*- Outside of specification <br />(1) The result for one or both determinations was less than five times the LOQ. <br />The background result was more than four times the spike added. <br />Lancaster Laboratories, Inc. <br />M E M B E R 2425 New Holland Pike <br />PO Box 12425 <br />Lancaster, 00 17605-2425 <br />Fax:77-6 <br />717-656-2300 Fax: 717-656-2681 <br />2216 Rev. 9/11/00 <br />