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• <br />i. Lancaster Laboratories <br />Mere quality is a science <br />Page 1 of 2 <br />Lancaster Laboratories Sample No. WPP 3761205 <br />Collected:01/17/2002 16:15 by DM Account Number: 10869 <br />Submitted: 01/19/2002 10:30 Chevron Products Company <br />Reported: 02/15/2002 at 13:17 6001 Bollinger Canyon Rd <br />Discard: 03/18/2002 Building L, Pp Box 6004 <br />EX -1-W-020117 Grab Water San Ramon CA 94583-0904 <br />Facility# 95775 SIRC <br />301 W Kettleman-Lodi 70607700839 EX -1 <br />WKEX1 <br />Lancaster Laboratories, Inc. <br />M E M B E R 2425 New Holland Pike <br />®PO Box 12425 <br />Lancaster, PA 17605-2425 <br />797-..- 2300 Fax: 717-656-2681 2216 Rev. 9/14100 <br />As Received <br />CAT <br />As Received <br />Method <br />Dilution <br />No. <br />Analysis Name <br />CAB Number <br />Result: <br />Detection <br />Units <br />Factor <br />Limit <br />01412 <br />Methanol and Ethanol <br />01414 <br />Methanol (by Direct Injection) <br />67-56-1 <br />N.D. <br />200. <br />ug/l <br />1 <br />1729 <br />TPH-GRO - Waters <br />01730 <br />TPH-GRO - Waters <br />n.a. <br />1,500. <br />250. <br />ug/1 <br />5 <br />The reported concentration of. <br />TPH-GRO does <br />not include MTBE or <br />other <br />gasoline constituents eluting <br />prior to the <br />C6 (n -hexane) TPH-GRD range <br />start time. <br />A site-specific MSD sample was <br />not submitted for the project. A <br />LCS/LCSD <br />was performed to demonstrate precision and <br />accuracy at a batch <br />level. <br />02159 <br />BTEX, MTBE <br />02161 <br />Benzene <br />71-43-2 <br />N.D. <br />2.5 <br />ug/l <br />5 <br />02164 <br />Toluene <br />108-88-3 <br />N.D. <br />2.5 <br />ug/l <br />5 <br />02166 <br />Ethylbenzene <br />100-41-4 <br />N.D. <br />2.5 <br />ug/l <br />5 <br />02171 <br />Total Xylenes <br />1330-20-7 <br />N.D. <br />7.5 <br />ug/l <br />5 <br />A site-specific MSD sample was <br />not submitted for the project. A <br />LCS/LCSD <br />was performed to demonstrate precision and <br />accuracy at a batch <br />level. <br />Due to dilution of the sample made. necessary by the high level <br />of non -target compounds, normal reporting limits were not <br />attained. <br />01594 <br />BTEX + Oxygenates by 8260B <br />01587 <br />Ethanol <br />64-17-5 <br />N.D. <br />1,300. <br />ug/1 <br />25 <br />02010 <br />Methyl t -butyl ether <br />1634-04-4 <br />25,000. <br />130. <br />ug/l <br />250 <br />02011 <br />di -Isopropyl ether <br />108-20-3 <br />N.D. <br />13. <br />ug/l <br />25 <br />02013 <br />Ethyl t -butyl ether <br />637-92-3 <br />760. <br />13. <br />ug/l <br />25 <br />014 <br />t -Amyl methyl ether <br />994-05-8 <br />250. <br />13. <br />ug/l <br />25 <br />.10 015 <br />t -Butyl alcohol <br />75-65-0 <br />390. <br />130. <br />ug/l <br />25 <br />Lancaster Laboratories, Inc. <br />M E M B E R 2425 New Holland Pike <br />®PO Box 12425 <br />Lancaster, PA 17605-2425 <br />797-..- 2300 Fax: 717-656-2681 2216 Rev. 9/14100 <br />