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Lancaster Laboratories <br />Where quality is a science. <br />Page] of 2 <br />Lancaster Laboratories Sample No. WW 3733567 <br />Collected:11/20/2001 14:49 by DM Account Number: 10869 <br />Submitted: 11/27/2001 10:00 Chevron Products Company <br />Reported: 12/11/2001 at 17:47 6001 Bollinger Canyon Rd <br />Discard: 01/11/2002 Building L, PO Box 6004 <br />MW -6-W-011120 NA Water San Ramon CA 94583-0904 <br />Facility# 95775 Prj.# 077.43449.650 SIRC <br />301 W. Kettleman Ln Lodi 70607700839 MW -6 <br />MW -6 - <br />As Received <br />CAT As Received Method Dilution <br />No. Analysis Name CAS Number Result Detection Units Factor <br />Limit <br />01412 Methanol and Ethanol <br />01414 Methanol (by Direct Injection} 67-56-1 N.D. 200. ug/1 I <br />01729 TPH-GRO - Waters <br />01730 TPH-GRO - Waters n.a. N.D. 50. ug/1 1 <br />The reported concentration of TPR-GRO does not include MTBE or other <br />gasoline constituents eluting prior to the C6 (n -hexane) TPH-GRO range <br />start time. <br />The vial submitted for volatile analysis did not have a pH < 2 at the time <br />of analysis. Due to the volatile nature of the analytes, it is not <br />appropriate for the laboratory to adjust the pH at the time of sample <br />receipt. <br />A site-specific MSD sample was not submitted for the project. A LCS/LCSD <br />was performed to demonstrate precision and accuracy at a batch level. <br />02159 BTEX, MT13E <br />02161 <br />Benzene <br />71-43-2 <br />N.D. <br />0.50 <br />ug/1 1 <br />02164 <br />Toluene <br />108-88-3 <br />N.D. <br />0.50 <br />ug/i 1 <br />02166 <br />Ethylbenzene' <br />100-41-4 <br />N.D. <br />0.50 <br />ug/l 1 <br />02171 <br />Total Xylenes <br />1330-20-7 <br />N.D. <br />1.5 <br />ug/l 1 <br />The vial submitted for volatile <br />analysis did <br />not have a pH < 2 <br />at the time <br />of analysis. Due to the volatile <br />nature of <br />the analytes, it is <br />not <br />appropriate for the laboratory <br />to adjust the <br />pH at the time of <br />sample <br />receipt. <br />A site-specific MSD sample was not submitted for the project. A LCS/LCSD <br />was performed to demonstrate precision and accuracy at a batch level. <br />�1&1594 BTEX + Oxygenates by 8260B <br />Lancaster Laboratories, Inc. <br />M E M B E R 2425 New Holland Pike <br />PO Box 12425 <br />Lancaster, 17605-2425 <br />717-656-230000 Fax: 717-6S6-2681 2216 Rev. 9111 <br />