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2425 New Hollai <br />Page 2 of 6 <br />*- Outside of specification <br />(1) The result for one or both determinations was less than five times the LOQ. <br />(2) The background result was more than four times the spike added. <br />..i <br />Quality <br />Control Summary <br />Client Name: ChevronTexaco <br />Group Number: <br />964517 <br />Reported: 11/04/05 at 10:23 AM <br />Laboratory <br />Compliance Quality <br />Control <br />Anal Name <br />Blank <br />Result <br />Blank Report LCS <br />MDL Units <br />LCSD <br />LCS/LCSD <br />1,2-Dichloroethane <br />N.D. <br />%REC <br />0.5 ug/1 110 <br />%REC <br />112 <br />Limits <br />RPD RPD Max <br />Toluene <br />N.D. <br />0.5 ug/1 92 <br />92 <br />77-132 <br />85-115 <br />2 30 <br />0 30 <br />1,2-Dibromoethane <br />N.D. <br />0.5 ug/l 92 <br />93 <br />81-114 <br />0 30 <br />Ethylbenzene <br />Xylene {Total) <br />N.D. <br />0.5 ug/l 96 <br />95 <br />82-119 <br />1 30 <br />N.D. <br />0.5 ug/l 96 <br />95 <br />83-113 <br />1 30 <br />Batch number: Z053043AA <br />Sample <br />number(s): 4631677-4631679 <br />Ethanol <br />Methyl Tertiary Butyl Ether <br />N.D. <br />N.D. <br />50. ug/l 84 <br />0.5 ug/l 107 <br />30-155 <br />di -Isopropyl ether <br />N.D. <br />0.5 ug/l a8 <br />77-127 <br />67-130 <br />Ethyl t -butyl ether <br />N.D. <br />0.5 ug/l 94 <br />74-120 <br />t -Amyl methyl ether <br />N.D. <br />0.5 ug/l 98 <br />79-113 <br />t -Butyl alcohol <br />N.D. <br />5. ug/l 97 <br />60-133 <br />Benzene <br />N.D. <br />0.5 ug/l 89 <br />85-117 <br />1,2-Dichloroethane <br />N.D. <br />0.5 ug/1 109 <br />77-132 <br />Toluene <br />N.D. <br />0.5 ug/l 91 <br />85-115 <br />1,2-Dibromoethane <br />N.D. <br />0.5 ug/l 91 <br />81-114 <br />I <br />Ethylbenzene <br />N.D. <br />0.5 ug/l 95 <br />82-119 <br />Xylene (Total) <br />N.D. <br />0.5 ug/l 96 <br />83-113 <br />rr <br />Sample Matrix Quality <br />Control <br />Analysis Name <br />MS <br />%REC <br />MSD M3/MSD RPD <br />%REC Limits RPD MAX <br />BKO <br />Conc <br />DUP <br />DUP Dup RPD <br />Conc <br />RPD Max <br />Batch number: 052990030A <br />Sample <br />number(s): 4631654-4631667 <br />Methanol (by Direct Injection) <br />98 <br />107 66-133 5 20 <br />Batch number: 05299AOBA <br />Sample <br />number(s): 4631653-4631662 <br />TPH-GRO - Waters_ <br />125 <br />63-154 <br />Batch number: 05299A16A <br />Sample <br />number(s); 4631663-4631674 <br />111 <br />TPH-GRO - Waters <br />120 <br />63-154 <br />Batch number: 053000025A <br />Sample <br />number(s): 4631668-4631679 <br />Methanol (by Direct Injection) <br />88 <br />88 66-133 0 20 <br />Batch number: 05301A16A <br />Sample <br />number(s): 4631675-4631679 <br />TPH-GRO - Waters <br />112 <br />63-154 <br />Batch number: Z052992AA <br />Sample <br />number(s): 4631653 <br />Methyl Tertiary Butyl Ether <br />116 <br />69-134 <br />Benzene <br />108 <br />83-128 <br />Toluene <br />111 <br />83-127 <br />Ethylbenzene <br />113 <br />82-129 <br />Xylene (Total) <br />111 <br />82-130 <br />�+ <br />Batch number: Z053021AA <br />Sample <br />number(s). 4631654-4631657 <br />Ethanol <br />91 <br />90 26-162 2 30 <br />Methyl Tertiary Butyl Ether <br />106 <br />105 69-134 1 30 <br />di -Isopropyl ether <br />96 <br />93 75-130 2 30 <br />r j <br />Ethyl t -butyl ether <br />98 <br />96 78-119 2 30 <br />j <br />t -Amyl methyl ether <br />99 <br />98 72-125 1 30 <br />*- Outside of specification <br />(1) The result for one or both determinations was less than five times the LOQ. <br />(2) The background result was more than four times the spike added. <br />..i <br />