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Lancaster - <br />. Laboratories n a 1 ys �. s Report <br />_5 New Holland Pike, PO Box 12425, Lancaster, PA 17605-2425 •717-656-2300 Fax: 717-656-2681 • www.lartbasterlabs.com <br />F Page 7 of 8 <br />Quality Control Summary <br />FClient Name: ChevronTexaco <br />Reported: 08/13/03 at 03:24 PM <br />Group Number: 861370 <br />Surrogate Quality Control <br />MSD 110 110 93 94 - <br />Limits: 81-120 82-112 - 85-112 83-113 <br />7 Analysis Name: BTEX+5 Oxygenates+EDC* EDB +ETON <br />Batch number: P032201AB <br />1 p i Dibromofluoromethane 1,2-Dichloroethane-d4 Toluene -d8 4-Bromofluorobenzene <br />VV76UzV <br />iV8 <br />109 <br />94 <br />90 <br />4092021 <br />109 <br />108 <br />94 <br />91 <br />4092022 <br />110 <br />107 <br />94 <br />92 <br />4092023 <br />111 <br />108 <br />93 <br />92 <br />"= 4092024 <br />110 <br />110 <br />94 <br />93 <br />4092025 <br />110 <br />109 <br />95 <br />92 <br />4092026 <br />111 <br />109 <br />93 <br />91 <br />1 4092027 <br />110 <br />111 <br />93 <br />91 <br />4092028 <br />111 <br />108 <br />95 <br />93. <br />4092029 <br />112 <br />110 <br />94 <br />93 <br />4092030 <br />109 <br />107 <br />93 <br />91 <br />4092031 <br />112 <br />108 <br />93 <br />92; <br />Blank <br />108 <br />106 <br />94 <br />93 <br />F, LCS <br />109 <br />110 <br />95 <br />96 <br />Ms <br />110 <br />111 <br />94 <br />95 <br />MSD <br />110 <br />110 <br />93 <br />94 <br />r <br />r <br />r <br />+ f' <br />Analysis Name: BTEX+5 Oxygenates+EDC+EDB+ETON <br />Batch number: P032211AA <br />Dibromofluoromethane 1,2-Dichloroethane-d4 Toluene -d8 <br />4-Bromofluorobenzene <br />4092032 <br />ts: 81-120 <br />82-112 <br />85-112 <br />83-113 <br />4092033 <br />"A.ialysis Name: BTEX+MTBE by 8260B <br />110 <br />95 <br />94 <br />4092034 <br />Batch number: P032202AA <br />.106 <br />95 <br />92 <br />4092035 <br />Dibromofluoromethane <br />1,2-Dichloroethane-d4 <br />Toluene -d8 <br />4-Bromofluorobenzene <br />Blank <br />108 <br />106 <br />94 <br />93 <br />II <br />4092018 103 <br />101 <br />89 <br />89 <br />._ <br />Blank 102 <br />98 <br />91 <br />91 <br />MSD <br />LCS 100 <br />98 <br />90 <br />93 <br />Limits: <br />MS 101 <br />102 <br />92 <br />94 <br />Analysis <br />MSD 102 <br />99 <br />90 <br />91 <br />Dibromofluoromethane <br />Limits: 81-120 <br />82-112 <br />B5-112 <br />83-113 <br />r <br />r <br />r <br />+ f' <br />Analysis Name: BTEX+5 Oxygenates+EDC+EDB+ETON <br />Batch number: P032211AA <br />Dibromofluoromethane 1,2-Dichloroethane-d4 Toluene -d8 <br />4-Bromofluorobenzene <br />4092032 <br />111 <br />105 <br />93 <br />90 <br />4092033 <br />110 <br />110 <br />95 <br />94 <br />4092034 <br />112 <br />.106 <br />95 <br />92 <br />4092035 <br />ill <br />106 <br />94 <br />92 <br />Blank <br />108 <br />106 <br />94 <br />93 <br />LCs <br />112 <br />107 <br />93 <br />94 <br />MS <br />92 <br />97 <br />101 <br />100 <br />MSD <br />95 <br />95 <br />100 <br />99 <br />Limits: <br />61-120 <br />82-112 <br />85-112 <br />83-113 <br />Analysis <br />Name: BTEX+5 Oxygenates +EDC+EDB+ETOH <br />Batch number: P032211AB <br />Dibromofluoromethane <br />1,2-Dichloroethane-d4 <br />Toluene -dB <br />4-Bromofluorobenzene <br />4092036 <br />108 <br />106 <br />101 <br />96 <br />*- Outside of specification <br />The result for one or bath determinations was less than five times the LOQ. <br />" The background result was more than four times the spike added. <br />