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ll <br />Batch number: 031960003A <br />F <br />Methanol (by Direct Injection) <br />Batch number: 03198A16A <br />TPH-GRO - Waters <br />Batch number: N032041AP <br />Ethanol <br />Lancaster <br />Methyl Tertiary Butyl Ether <br />t <br />di -Isopropyl ether <br />Ethyl t -butyl ether <br />t -Amyl methyl ether <br />Laboratories <br />F <br />Benzene <br />Analysis <br />Report <br />2425 New Holland Pike, PO Box 12425, Lancaster, PA 17605-2425 •717.656-2300 Fax 717-656-2681 • www.lanoa6terfabs.com <br />FPage <br />] of 3 <br />Quality <br />Control <br />Summary <br />Client Name; ChevronTexaco <br />Group <br />Number: 859631 <br />Reported: 07/27/03 at 11:20 <br />AM <br />Laboratory <br />Compliance Quality Control <br />W <br />Analysis Name <br />Blank <br />Result <br />Blank <br />MAL <br />Report <br />Units <br />LCS <br />RSC <br />LCSD LCS/LCSD <br />$RSC Limits <br />RPD RPD Max <br />Batch number: 031980003A <br />Sample <br />number(s): <br />4082976-4082980 <br />Methanol (by Direct Injection) <br />N.D. <br />200. <br />ug/l <br />88 <br />78-114 <br />Batch number: 0319BA16A <br />Sample <br />number(s): <br />4082976-4082980 <br />TPH-GRO - Waters <br />N.D. <br />50. <br />ug/l <br />111 <br />115 70-130 <br />4 30 <br />r--� <br />Batch number: N032041AB <br />Sample <br />number(s): <br />4082980 <br />Ethanol <br />Methyl Tertiary Butyl Ether <br />N.D. <br />N.D. <br />50. <br />0.5 <br />ug/l <br />ug/l <br />84 <br />102 <br />43-159 <br />di -Isopropyl ether <br />N.D. <br />0.5 <br />ug/l <br />103 <br />77-127 <br />74-125 <br />Ethyl t -butyl ether <br />t -Amyl methyl ether <br />N.D. <br />N.D. <br />0.5 <br />ug/1 <br />90 <br />74-120 <br />t -Butyl alcohol <br />N.D. <br />0.5 <br />51 <br />ug/l <br />ug/l <br />91 <br />82 <br />79-113 <br />Benzene <br />1,2-Dichloroethane <br />N.D. <br />0.5 <br />ug/l <br />110 <br />53-147 <br />85-117 <br />Toluene <br />N.D. <br />N.D. <br />0.5 <br />0.5 <br />ug/l <br />ug/l <br />107 <br />109 <br />77-132 <br />1,2-Dibromoethane <br />N.D. <br />0.5 <br />ug/l <br />98 <br />85-115 <br />81-114 <br />('^ <br />Ethylbenzene <br />Xylene (Total) <br />N.D. <br />0.5 <br />ug/l <br />108 <br />82-119 <br />N.D. <br />0.5 <br />ug/l <br />110 <br />84-120 <br />Y i <br />Batch number: P032031AA <br />Sample <br />number(s): <br />4082976-4082979 <br />Ethanol <br />Methyl Tertiary Butyl Ether <br />N.D. <br />N.D. <br />50. <br />0.5 <br />ug/l <br />ug/l <br />94 <br />95 <br />43-159 <br />Fdi-Isopropyl <br />ether <br />N.D. <br />0.5 <br />ug/l <br />98 <br />77-127 <br />74-125 <br />,,,.Ethyl <br />t -butyl ether <br />N.D. <br />0.5 <br />ug/1 <br />97 <br />74-120 <br />t -Amyl methyl ether <br />N.D. <br />0.5 <br />ug/l <br />93 <br />79-113 <br />t -Butyl alcohol <br />Benzene <br />N.D. <br />5. <br />ug/l <br />98 <br />53-147 <br />1,2-Dichloroethane <br />N.D. <br />N.D. <br />0.5 <br />0.5 <br />ug/l <br />ug/l <br />95 <br />99 <br />85-117 <br />F <br />Toluene <br />N.D. <br />0.5 <br />ug/l <br />96 <br />77-132 <br />85-115 <br />1, 2 -Dibromoethane <br />Ethylbenzene <br />N.D. <br />0.5 <br />ug/l <br />94 <br />8I-114 <br />Xylene (Total) <br />N.D. <br />N.D. <br />0.5 <br />0.5 <br />ug/l <br />ug/l <br />95 <br />96 <br />82-119 <br />84-120 <br />FAnalysis Name <br />Sample Matrix Quality Control <br />MS MSD MS/MSD RPD BKG DUP <br />REC %REC Limits RPD KhX cone Conc <br />Sample number(s): 4082976-4082980 <br />8s 88 78-116 0 20 <br />Sample number(s): 4082976-4082980 <br />119 70-130 <br />Sample number(s): 4082980 <br />83 81 34-163 2 30 <br />97 92 69-134 2 30 <br />106 104 75-130 2 30 <br />91 90 73-123 2 30 <br />93 92 77-117 1 30 <br />82 81 39-155 1 30 <br />115 113 83-128 2 30 <br />*- Outside of specification <br />7 (1) The result for one or both determinations was less than five times the LOQ. <br />.1 (2) The background result was more than four times the spike added. <br />II <br />DUP <br />RPD <br />Dup <br />RPD <br />Max <br />Batch number: 031960003A <br />F <br />Methanol (by Direct Injection) <br />Batch number: 03198A16A <br />TPH-GRO - Waters <br />Batch number: N032041AP <br />Ethanol <br />Methyl Tertiary Butyl Ether <br />t <br />di -Isopropyl ether <br />Ethyl t -butyl ether <br />t -Amyl methyl ether <br />t -Butyl alcohol <br />F <br />Benzene <br />Sample Matrix Quality Control <br />MS MSD MS/MSD RPD BKG DUP <br />REC %REC Limits RPD KhX cone Conc <br />Sample number(s): 4082976-4082980 <br />8s 88 78-116 0 20 <br />Sample number(s): 4082976-4082980 <br />119 70-130 <br />Sample number(s): 4082980 <br />83 81 34-163 2 30 <br />97 92 69-134 2 30 <br />106 104 75-130 2 30 <br />91 90 73-123 2 30 <br />93 92 77-117 1 30 <br />82 81 39-155 1 30 <br />115 113 83-128 2 30 <br />*- Outside of specification <br />7 (1) The result for one or both determinations was less than five times the LOQ. <br />.1 (2) The background result was more than four times the spike added. <br />II <br />DUP <br />RPD <br />Dup <br />RPD <br />Max <br />