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Lancaster <br />V Laboratories Analysis Report <br />2425 New Holland Pike, PO Box 12425, L&nCaster, PA 1 76 05-242 5 •717-656-2300 Fax: 717-656-2681 • W W WAancasterlabs,com <br />Analysis Name: BTEX+5 Oxygenates+SDC+EDB+ETOH <br />Batch number: P032031AA <br />Dibromofluoromethane <br />1,2-Dichloroethane-d4 <br />Page 3 of 3 <br />4-Bromofluorobenzene <br />Quality Control Summary <br />95 <br />Client Name: <br />ChevronTexaco <br />Group Number: 859631 <br />4082977 <br />Reported: <br />07/27/03 at 11:20 AM <br />93 <br />4082978 <br />Surrogate <br />Quality Control <br />100 <br />Limits: <br />57-146 <br />94 <br />96 <br />Analysis Name: BTEX+5 Oxygenates+EDC+EDB+ETOH <br />94 <br />Blank <br />Batch number: N032041AB <br />93 <br />102 <br />95 <br />Dibromofluoromethane 1,2-Dichloroethane-d4 <br />Toluene -d8 <br />4-Bromofluorobenzene <br />4082980 <br />Blank <br />100 93 <br />100 <br />100 <br />94 <br />MCS <br />9693 <br />100 <br />100 <br />94 <br />MS <br />MSD <br />97 <br />96 95 <br />99 100 <br />100 <br />99 <br />Limits: <br />81-120 82-112 <br />85-112 <br />83-113 <br />Analysis Name: BTEX+5 Oxygenates+SDC+EDB+ETOH <br />Batch number: P032031AA <br />98 <br />Limits: e1-120 82-112 <br />85-112 83-113 <br />�k <br />i <br />*- Outside of specification <br />(1) The result for one or both determinations was less than five times the LOQ. <br />(2) The background result was more than four times the spike added. <br />Dibromofluoromethane <br />1,2-Dichloroethane-d4 <br />Toluene -d8 <br />4-Bromofluorobenzene <br />4082976 <br />95 <br />92 <br />100 <br />4082977 <br />95 <br />96 <br />93 <br />4082978 <br />97 <br />93 <br />100 <br />92 <br />4082979 <br />94 <br />96 <br />101 <br />94 <br />Blank <br />95 <br />93 <br />102 <br />95 <br />LCS <br />94 <br />111 <br />94 <br />MS <br />94 <br />95 <br />97 <br />99 <br />MSD <br />9596 <br />98 <br />95 <br />99 <br />98 <br />Limits: e1-120 82-112 <br />85-112 83-113 <br />�k <br />i <br />*- Outside of specification <br />(1) The result for one or both determinations was less than five times the LOQ. <br />(2) The background result was more than four times the spike added. <br />