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r <br />Lancaster <br />Laboratories Analysis Report <br />✓ 2425 New Holland Pike, PO Box 12425, Lancaster, PA 17605.2425 717-656-2300 Fax: 717-6562681 • www,lancasterlabs.com <br />State of California Lab Certification No. 2116 <br />Trip blank vials were not received by the laboratory for this sample group. <br />Laboratory <br />Chronicle <br />Page 1 of 2 <br />Lancaster Laboratories Sample <br />No. WW 4107519 <br />Analysis <br />Trial# Date and Time <br />Dilution <br />Analyst Factor <br />01728 TPH-GRO - Waters <br />N. CA LUFT Gasoline <br />F <br />Collected:08/20/2003 00:00 <br />by GC <br />Method <br />SW -846 6OlSe <br />Account Number: <br />10869 <br />Submitted: 08/22/2003 09:30 <br />F <br />ChevronTexaco <br />Reported: 09/02/2003 at 16:03 <br />6001 Bollinger <br />Canyon Rd <br />L4310 <br />Discard: 10/03/2003 <br />INF -W-030820 Grab <br />Water <br />San Ramon CA <br />94583 <br />Facility# 95775 <br />SIM <br />301 W Kettleman Lodi T0607700839 NA <br />LOINF <br />As Received <br />CAT <br />As Received Method <br />Dilution <br />No. Analysis Name <br />CAB Number <br />Result <br />Detection <br />Units <br />Factor <br />01728 TPH-GRO - Waters <br />n.a. <br />N.D. <br />Limit <br />50. <br />119/1 <br />1 <br />The reported concentration of <br />TPH-GRO does not include <br />MTBE or other <br />gasoline constituents eluting <br />prior to the C6 <br />(n -hexane} TPH-GRO range <br />start time. <br />` <br />A site-specific MSD sample was not submitted <br />for the project. A LCS/LCSD <br />was performed to demonstrate precision and accuracy <br />at <br />a batch level. <br />�-^ <br />I <br />01412 Methanol and Ethanol <br />01414 Methanol (by Direct Injection) <br />67-56-1 <br />N.D. <br />400. <br />ug/l <br />1 <br />The percent recovery for methanol <br />was outside <br />QC limits <br />in the <br />LCS associated with this sample. <br />This compound met recovery <br />criteria <br />in the MS/MSD analysis. <br />01594 BTEX+S oxygenates+EDC+EDB+ETOH <br />01587 Ethanol <br />64-17-5 <br />N.D. <br />100. <br />ug/1 <br />1 <br />02010 Methyl Tertiary Butyl Ether <br />1634-04-4 <br />9. <br />2. <br />ug/1 <br />1 <br />02011 di -Isopropyl ether <br />108-20-3 <br />N.D. <br />2. <br />ug/l <br />1 <br />02013 Ethyl t -butyl ether <br />637-92-3 <br />N D <br />2 <br />ug/1 <br />1 <br />02014 t -Amyl methyl ether <br />994-05-8 <br />N.D. <br />2• <br />ug/1 <br />1 <br />02015 t -Butyl alcohol <br />75-65-0 <br />N.D. <br />10. <br />ug/1 <br />1 <br />05401 Benzene <br />71-43-2 <br />N.D. <br />2. <br />ug/l <br />F <br />05402 1,2-Dichloroethane <br />107-06-2 <br />N.D. <br />2. <br />ug/l <br />1 <br />05407 Toluene <br />108-88-3 <br />N,D. <br />2. <br />ug/l <br />1 <br />05412 1,2-Dibromoethane <br />106-93-4 <br />N.D. <br />2. <br />ug/l <br />1 <br />05415 Ethylbenzene <br />100-41-4 <br />N.D. <br />2. <br />ug/l <br />1 <br />06310 Xylene (Total} <br />1330-20-7 <br />N.D. <br />2. <br />ug/l <br />1 <br />State of California Lab Certification No. 2116 <br />Trip blank vials were not received by the laboratory for this sample group. <br />Laboratory <br />Chronicle <br />CAT <br />No. Analysis Name <br />Method <br />Analysis <br />Trial# Date and Time <br />Dilution <br />Analyst Factor <br />01728 TPH-GRO - Waters <br />N. CA LUFT Gasoline <br />1 08/26/2003 04:26 <br />Victoria M Martell 1 <br />01412 Methanol and Ethanol <br />Method <br />SW -846 6OlSe <br />1 08/29/2003 18:15 <br />Lisa A Johnson 1 <br />F <br />